2,4(1H,3H)-Pyrimidinedione, 5-bromo-6-methyl-1-phenyl-3-(2-propenyl)-

Base Information

• Chemical Name: 2,4(1H,3H)-Pyrimidinedione, 5-bromo-6-methyl-1-phenyl-3-(2-propenyl)-
• CAS No.: 32000-77-4
• Molecular Formula: C14H13 Br N2 O2
• Molecular Weight: 321.17
• Hs Code.: 2933599090
• Mol file: 32000-77-4.mol

Synonyms:2,4(1H,3H)-Pyrimidinedione,5-bromo-6-methyl-1-phenyl-3-(2-propenyl)- (9CI); Uracil,3-allyl-5-bromo-6-methyl-1-phenyl- (8CI);3-Allyl-5-bromo-6-methyl-1-phenyluracil

Chemical Property of 2,4(1H,3H)-Pyrimidinedione, 5-bromo-6-methyl-1-phenyl-3-(2-propenyl)-

Chemical Property:

• Vapor Pressure: 4.92E-06mmHg at 25°C
• Boiling Point: 381.9°Cat760mmHg
• Flash Point: 184.7°C
• PSA: 44.00000
• Density: 1.469g/cm³
• LogP: 2.25610

Purity/Quality:

2,4(1H,3H)-PYRIMIDINEDIONE, 5-BROMO-6-METHYL-1-PHENYL-3-(2-PROPENYL)- 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4(1H,3H)-Pyrimidinedione, 5-bromo-6-methyl-1-phenyl-3-(2-propenyl)-

There total 1 articles about 2,4(1H,3H)-Pyrimidinedione, 5-bromo-6-methyl-1-phenyl-3-(2-propenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3-allyl-5-bromo-6-methyl-1-phenyl-1H-pyrimidine-2,4-dione (32000-77-4)

Guidance literature:

5-Brom-1-phenyl-6-methyl-uracil, Na-Ethylat, abs. Ethanol, Allylbromid, Erhitzen;

DOI:10.1021/jm00275a008

Reference yield: 59.0%

3-allyl-5-bromo-6-methyl-1-phenyl-1H-pyrimidine-2,4-dione (32000-77-4) → 4-(3-allyl-1-phenylureido)-5-methylpyrazol-3(2H)-one (85349-85-5)

Guidance literature:

With hydrazine hydrate; In isopropyl alcohol; for 24h; Heating;

Reference yield: 19.0%

3-allyl-5-bromo-6-methyl-1-phenyl-1H-pyrimidine-2,4-dione (32000-77-4) → 3-allyl-1-phenylhydantoin (55889-18-4)

Guidance literature:

With methylamine; In N,N-dimethyl-formamide; at 100 ℃; for 18h;

Downstream raw materials:

3-allyl-1-phenylhydantoin

4-(3-allyl-1-phenylureido)-5-methylpyrazol-3(2H)-one

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