Technology Process of Yttrium phosphide
There total 2 articles about Yttrium phosphide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
neat (no solvent);
heating Y and red P in a sealed quartz ampoule at 1100°C for 20 h under pressure of 6.6E-3 Pa, rate of raising temp. from 300 to 1100°C less than 1°C/min., regrinding, pelleting, sintering at 1100°C for 10 h and 6.6E-3 Pa;
- Guidance literature:
-
In
neat (no solvent, solid phase);
stoich. proportions mixed, evacuated, sealed in quartz ampoules under 6.6E-3 Pa, heated at 1100°C for 20 h, reground, pressed into pellets, evacuated, sealed under 6.6E-3 Pa, sintered at 1100°C for 10 h; carrier conc. 5.5E17 cm-3;
DOI:10.1016/0038-1098(91)90056-2
