3,6-Dimethoxy-9-phenyl-9h-fluorene

Base Information

Chemical Name:3,6-Dimethoxy-9-phenyl-9h-fluorene
CAS No.:6162-04-5
Molecular Formula:C₂₁H₁₈O₂
Molecular Weight:302.373
Hs Code.:
NSC Number:86547
DSSTox Substance ID:DTXSID20292945
Wikidata:Q82031463

Synonyms:6162-04-5;3,6-dimethoxy-9-phenyl-9h-fluorene;NSC86547;DTXSID20292945;NSC-86547

Suppliers and Price of 3,6-Dimethoxy-9-phenyl-9h-fluorene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3,6-Dimethoxy-9-phenyl-9h-fluorene

Chemical Property:

Vapor Pressure:8.09E-08mmHg at 25°C
Boiling Point:448.6°Cat760mmHg
Flash Point:176°C
Density:1.16g/cm³
XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:302.130679813
Heavy Atom Count:23
Complexity:361

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC2=C(C=C1)C(C3=C2C=C(C=C3)OC)C4=CC=CC=C4

Technology Process of 3,6-Dimethoxy-9-phenyl-9h-fluorene

There total 5 articles about 3,6-Dimethoxy-9-phenyl-9h-fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119-90-4
3,3'-dimethoxy-(1,1'-biphenyl)-4,4'-diamine

: 6162-04-5
3,6-Dimethoxy-9-phenyl-fluoren

Guidance literature:: Multi-step reaction with 4 steps

1: Br₂ / acetic acid

2: aq. KOH, EtOH

3: aq. NaNO₂, aq. H₃PO₂

4: (i) Mg, (ii) /BRN= 471223/, (iii) polyphosphoric acid

With potassium hydroxide; ethanol; bromine; hypophosphorous acid; sodium nitrite; In acetic acid;

Reference yield:

: 14344-81-1
2-bromo-5,3'-dimethoxy-benzidine

: 6162-04-5
3,6-Dimethoxy-9-phenyl-fluoren

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaNO₂, aq. H₃PO₂

2: (i) Mg, (ii) /BRN= 471223/, (iii) polyphosphoric acid

With hypophosphorous acid; sodium nitrite;

Reference yield:

: 14344-80-0
N,N'-(2-bromo-5,3'-dimethoxy-biphenyl-4,4'-diyl)-bis-acetamide

: 6162-04-5
3,6-Dimethoxy-9-phenyl-fluoren

Guidance literature:: Multi-step reaction with 3 steps

1: aq. KOH, EtOH

2: aq. NaNO₂, aq. H₃PO₂

3: (i) Mg, (ii) /BRN= 471223/, (iii) polyphosphoric acid

With potassium hydroxide; ethanol; hypophosphorous acid; sodium nitrite;