(NE)-N-[(6-phenyl-2,3-dihydroimidazo[2,1-b][1,3]thiazol-5-yl)methylidene]hydroxylamine

Base Information

• Chemical Name: (NE)-N-[(6-phenyl-2,3-dihydroimidazo[2,1-b][1,3]thiazol-5-yl)methylidene]hydroxylamine
• CAS No.: 83253-33-2
• Molecular Formula: C12H11N3OS
• Molecular Weight: 245.3002
• NSC Number: 332753
• DSSTox Substance ID: DTXSID80429790

Synonyms:NSC332753;83253-33-2;(NE)-N-[(6-phenyl-2,3-dihydroimidazo[2,1-b][1,3]thiazol-5-yl)methylidene]hydroxylamine;DTXSID80429790;HMS1449H01;CCG-250580;NSC-332753;IDI1_017878

Chemical Property of (NE)-N-[(6-phenyl-2,3-dihydroimidazo[2,1-b][1,3]thiazol-5-yl)methylidene]hydroxylamine

Chemical Property:

• Vapor Pressure: 3.99E-11mmHg at 25°C
• Boiling Point: 507.6°Cat760mmHg
• Flash Point: 260.8°C
• Density: 1.42g/cm³
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 245.06228316
• Heavy Atom Count: 17
• Complexity: 294

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CSC2=NC(=C(N21)C=NO)C3=CC=CC=C3
• Isomeric SMILES: C1CSC2=NC(=C(N21)/C=N/O)C3=CC=CC=C3

Technology Process of (NE)-N-[(6-phenyl-2,3-dihydroimidazo[2,1-b][1,3]thiazol-5-yl)methylidene]hydroxylamine

There total 2 articles about (NE)-N-[(6-phenyl-2,3-dihydroimidazo[2,1-b][1,3]thiazol-5-yl)methylidene]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-diidro-5-formil-6-fenilimidazo<2,1-b>tiazolo (75224-64-5) → 6-Phenyl-2,3-dihydro-imidazo[2,1-b]thiazole-5-carbaldehyde oxime (83253-33-2)

Guidance literature:

With ammonium hydroxide; hydroxylamine hydrochloride; In ethanol; for 0.166667h; Yield given; Heating;

Reference yield:

2,3-diidro-6-fenilimidazo<2,1-b>tiazolo (4335-28-8) → 6-Phenyl-2,3-dihydro-imidazo[2,1-b]thiazole-5-carbaldehyde oxime (83253-33-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trichlorophosphate / chloroform / 0 - 5 °C

1.2: 5 h / Reflux

2.1: hydroxylamine hydrochloride; ammonium hydroxide / ethanol; water / 0.17 h / pH 6 / Reflux

With ammonium hydroxide; hydroxylamine hydrochloride; trichlorophosphate; In ethanol; chloroform; water;

DOI:10.2174/1573406413666171010110819

Reference yield:

6-Phenyl-2,3-dihydro-imidazo[2,1-b]thiazole-5-carbaldehyde oxime (83253-33-2) → 6-Phenyl-2,3-dihydro-imidazo[2,1-b]thiazole-5-carbonitrile (83253-38-7)

Guidance literature:

With selenium(IV) oxide; In chloroform; N,N-dimethyl-formamide; for 4h; Yield given; Heating;

upstream raw materials:

2,3-diidro-5-formil-6-fenilimidazo<2,1-b>tiazolo

2,3-diidro-6-fenilimidazo<2,1-b>tiazolo

Downstream raw materials:

6-Phenyl-2,3-dihydro-imidazo[2,1-b]thiazole-5-carbonitrile

6-Phenyl-2,3-dihydro-imidazo[2,1-b]thiazole-5-carboxylic acid amide

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