5-(3,4-Dimethyl-2-phenyldiazenylanilino)pentane-1,2,3,4-tetrol

Base Information

• Chemical Name: 5-(3,4-Dimethyl-2-phenyldiazenylanilino)pentane-1,2,3,4-tetrol
• CAS No.: 21037-25-2
• Molecular Formula: C19H25N3O4
• Molecular Weight: 359.425
• European Community (EC) Number: 244-162-2
• ChEMBL ID: CHEMBL1417630
• Mol file: 21037-25-2.mol

Synonyms:MLS000709088;SMR000282955;cid_89417;CHEMBL1417630;BDBM33880;HMS2770F16;21037-25-2;5-(3,4-dimethyl-2-phenyldiazenylanilino)pentane-1,2,3,4-tetrol;EINECS 244-162-2;AKOS000659738;NCGC00245464-01;SR-01000314654;SR-01000762135;SR-01000314654-1;SR-01000762135-2;1-Deoxy-1-(2-(phenylazo)-3,4-xylidino)-D-ribitol;5-(3,4-dimethyl-2-phenylazo-anilino)pentane-1,2,3,4-tetrol;5-[(3,4-dimethyl-2-phenyldiazenyl-phenyl)amino]pentane-1,2,3,4-tetrol

Chemical Property of 5-(3,4-Dimethyl-2-phenyldiazenylanilino)pentane-1,2,3,4-tetrol

Chemical Property:

• Vapor Pressure: 1.08E-17mmHg at 25°C
• Boiling Point: 648.3°Cat760mmHg
• Flash Point: 345.9°C
• PSA: 117.67000
• Density: 1.27g/cm³
• LogP: 2.27870
• XLogP3: 2.4
• Hydrogen Bond Donor Count: 5
• Hydrogen Bond Acceptor Count: 7
• Rotatable Bond Count: 8
• Exact Mass: 359.18450629
• Heavy Atom Count: 26
• Complexity: 431

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C(=C(C=C1)NCC(C(C(CO)O)O)O)N=NC2=CC=CC=C2)C

Technology Process of 5-(3,4-Dimethyl-2-phenyldiazenylanilino)pentane-1,2,3,4-tetrol

There total 2 articles about 5-(3,4-Dimethyl-2-phenyldiazenylanilino)pentane-1,2,3,4-tetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzenediazonium (2684-02-8) + 3,4-dimethyl-N-ribitylaniline (3051-94-3) → N-<3,4-dimethyl-6-(phenylazo)phenyl>-D-ribitylamine (21037-26-3) + N-<3,4-dimethyl-2-(phenylazo)phenyl>-D-ribitylamine (21037-25-2)

Guidance literature:

DOI:10.1021/ja01198a068 DOI:10.1002/hlca.19360190141

Reference yield:

benzenediazonium (2684-02-8) + L-ribo-5-(3.4-dimethyl-anilino)-1.2.3.4-tetraacetoxy-pentane (911650-71-0) → N-<3,4-dimethyl-6-(phenylazo)phenyl>-D-ribitylamine (21037-26-3) + N-<3,4-dimethyl-2-(phenylazo)phenyl>-D-ribitylamine (21037-25-2)

Guidance literature:

und Behandlung des Reaktionsprodukts mit Natriummethylat in Methanol;

DOI:10.1021/ja01198a068

Reference yield:

N-<3,4-dimethyl-2-(phenylazo)phenyl>-D-ribitylamine (21037-25-2) → 6,7-dimethyl-10-D-ribitol-1-yl-10H-benzo[g]pteridine-2,4-dione (5984-80-5)

Guidance literature:

bei der Reduktion und anschliessenden Umsetzung des Reaktionsprodukts mit Alloxan in Essigsaeure unter Zusatz von H₃BO₃;

DOI:10.1021/ja01198a068

upstream raw materials:

benzenediazonium

3,4-dimethyl-N-ribitylaniline

L-ribo-5-(3.4-dimethyl-anilino)-1.2.3.4-tetraacetoxy-pentane

Downstream raw materials:

1-(2-amino-3,4-dimethyl-anilino)-D-1-deoxy-ribitol

6,7-dimethyl-10-D-ribitol-1-yl-10H-benzo[g]pteridine-2,4-dione