Mucochloric acid isopropyl ether

Base Information

• Chemical Name: Mucochloric acid isopropyl ether
• CAS No.: 29814-12-8
• Molecular Formula: C7H8 Cl2 O3
• Molecular Weight: 211.045
• DSSTox Substance ID: DTXSID001031189
• Mol file: 29814-12-8.mol

Synonyms:Mucochloric acid isopropyl ether;29814-12-8;CCRIS 6598;DTXSID001031189

Chemical Property of Mucochloric acid isopropyl ether

Chemical Property:

• Vapor Pressure: 0.00738mmHg at 25°C
• Boiling Point: 269.1°Cat760mmHg
• Flash Point: 112.7°C
• Density: 1.308g/cm³
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 209.9850495
• Heavy Atom Count: 12
• Complexity: 221

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)OC(=O)C(=C(C=O)Cl)Cl
• Isomeric SMILES: CC(C)OC(=O)/C(=C(\C=O)/Cl)/Cl

Technology Process of Mucochloric acid isopropyl ether

There total 4 articles about Mucochloric acid isopropyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

Mucochloric acid (766-40-5) → 3,4-dichloro-5-isopropyloxy-2(5H)-furanone (29814-12-8)

Guidance literature:

With sulfuric acid; In isopropyl alcohol; toluene; for 18h; Dean-Stark; Inert atmosphere; Resolution of racemate;

DOI:10.15227/orgsyn.069.0205

Reference yield: 82.0%

Mucochloric acid (766-40-5) + isopropyl alcohol (67-63-0,8013-70-5) → 3,4-dichloro-5-isopropyloxy-2(5H)-furanone (29814-12-8)

Guidance literature:

With sulfuric acid; In toluene; Reflux;

DOI:10.1016/j.ejmech.2018.03.021

Reference yield: 73.0%

mucochloric acid (87-56-9) + isopropyl alcohol (67-63-0,8013-70-5) → 3,4-dichloro-5-isopropyloxy-2(5H)-furanone (29814-12-8)

Guidance literature:

With sulfuric acid; for 48h; Reflux;

DOI:10.1002/ardp.201600036

upstream raw materials:

Mucochloric acid

isopropyl alcohol

mucochloric acid