4-ACETYLAMINO-6-DIAZO-2,4-CYCLOHEXADIENONE

Base Information

• Chemical Name: 4-ACETYLAMINO-6-DIAZO-2,4-CYCLOHEXADIENONE
• CAS No.: 98555-06-7
• Molecular Formula: C8H7 N3 O2
• Molecular Weight: 177.162
• Hs Code.: 2927000090
• Mol file: 98555-06-7.mol

Synonyms:4-ACETYLAMINO-6-DIAZO-2,4-CYCLOHEXADIENONE

Chemical Property of 4-ACETYLAMINO-6-DIAZO-2,4-CYCLOHEXADIENONE

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 82.71000
• Density: g/cm³
• LogP: 1.12740

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-ACETYLAMINO-6-DIAZO-2,4-CYCLOHEXADIENONE

There total 2 articles about 4-ACETYLAMINO-6-DIAZO-2,4-CYCLOHEXADIENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-acetaminophenol (103-90-2,8055-08-1) → N-acetyl-p-benzoquinoneimine (50700-49-7) + 4-acetylamino-6-diazo-2,4-cyclohexadienone (98555-06-7) + N-(4-hydroxy-3-nitrophenyl)acetamide (51288-37-0) + 2,6-dinitro-4-acetylaminophenol (118828-85-6) + p-benzoquinone (106-51-4)

Guidance literature:

With dinitrogen trioxide; at 37 ℃; for 1h; Product distribution; pH 3; under model stomach conditions; var. nitrite concn.s;

DOI:10.1248/cpb.36.4634

Reference yield:

→ 4-acetylamino-6-diazo-2,4-cyclohexadienone (98555-06-7)

Guidance literature:

3-Amino-4-hydroxy-acetanilid in verd. HCl, Diazotierung m. NaNO2 bei 4grad;

DOI:10.1021/jo01060a006

upstream raw materials:

4-acetaminophenol

Refernces