quinolinium hydrogen sulphate

Base Information

• Chemical Name: quinolinium hydrogen sulphate
• CAS No.: 530-66-5
• Molecular Formula: C9H9NO4S
• Molecular Weight: 227.241
• Hs Code.: 2933499090
• Mol file: 530-66-5.mol

Synonyms:Quinoline sulfate (1:1);Quinoline bisulfate;Quinolinium hydrogen sulphate;

Chemical Property of quinolinium hydrogen sulphate

Chemical Property:

• Vapor Pressure: 0.0822mmHg at 25°C
• Melting Point: 162-164 °C
• Boiling Point: 234.1 °C at 760 mmHg
• Flash Point: 101.1 °C
• PSA: 95.87000
• LogP: 2.66280
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

98%min ^*data from raw suppliers

quinoliniumhydrogensulphate 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of quinolinium hydrogen sulphate

There total 4 articles about quinolinium hydrogen sulphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

quinoline (91-22-5) → Quinoline sulfate (530-66-5)

Guidance literature:

With sulfuric acid; In ethanol; at 5 - 20 ℃; for 2h; Temperature;

Reference yield:

quinoline (91-22-5) → bis-quinolinium sulphate (530-66-5,41949-04-6,54957-90-3)

Guidance literature:

With sulfuric acid; at 20 ℃;

DOI:10.1016/j.chemphys.2010.07.007

Reference yield:

sulfuric acid (7664-93-9) + 1-(2,3,4-trihydroxy-phenacyl)-quinolinium; chloride (53420-91-0) → formyl chloride (2565-30-2) + bis-quinolinium sulphate (530-66-5,41949-04-6,54957-90-3)

Guidance literature:

upstream raw materials:

sulfuric acid

1-(2,3,4-trihydroxy-phenacyl)-quinolinium; chloride

1-(3',4'-dihydroxyphenacyl)quinolinium chloride

quinoline

Downstream raw materials:

8-quinolinesulfonic acid

Refernces

• 1、 Bouchouit,Bendeif,El Ouazzani,Dahaoui,Lecomte,Benali-Cherif,Sahraoui. "Correlation between structural studies and third order NLO properties of selected new quinolinium semi-organic compounds". experimental part. p. 1 - 7. Retrieved 2011/01/06.