Cyclohexanone, 2-(9-phenanthrenyl)-

Base Information

Chemical Name:Cyclohexanone, 2-(9-phenanthrenyl)-
CAS No.:73129-94-9
Molecular Formula:C20H18O
Molecular Weight:274.362
Hs Code.:
DSSTox Substance ID:DTXSID70993874
Nikkaji Number:J3.379.623D

Synonyms:73129-94-9;Cyclohexanone, 2-(9-phenanthrenyl)-;DTXSID70993874;2-(PHENANTHREN-9-YL)CYCLOHEXAN-1-ONE

Suppliers and Price of Cyclohexanone, 2-(9-phenanthrenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Cyclohexanone, 2-(9-phenanthrenyl)-

Chemical Property:

Vapor Pressure:1.36E-09mmHg at 25°C
Boiling Point:485.9°Cat760mmHg
Flash Point:216.2°C
Density:1.165g/cm³
XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:274.135765193
Heavy Atom Count:21
Complexity:387

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(=O)C(C1)C2=CC3=CC=CC=C3C4=CC=CC=C42

Technology Process of Cyclohexanone, 2-(9-phenanthrenyl)-

There total 5 articles about Cyclohexanone, 2-(9-phenanthrenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 111189-35-6
2-(9-phenanthryl)cyclohexanol

: 73129-94-9
2-(phenanthren-9-yl)cyclohexanone

Guidance literature:: With dipyridinium dichromate; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1021/jo00235a005

Reference yield: 64.0%

: 573-17-1
9-bromophenanthrene

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 73129-94-9
2-(phenanthren-9-yl)cyclohexanone

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; caesium carbonate; In toluene; at 110 ℃; Inert atmosphere;
DOI:10.1021/jo501576e

Reference yield:

: 573-17-1
9-bromophenanthrene

: 73129-94-9
2-(phenanthren-9-yl)cyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyllithium / 1.) hexane, ether, 2 h, 2.) ether, overnight

2: 88 percent / pyridinium dichromate / dimethylformamide / Ambient temperature

With dipyridinium dichromate; n-butyllithium; In N,N-dimethyl-formamide;
DOI:10.1021/jo00235a005