Technology Process of phenanthro[9,10-g]isoquinoline
There total 6 articles about phenanthro[9,10-g]isoquinoline which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
PPA;
at 130 ℃;
for 8h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 92 percent / aluminum chloride / nitrobenzene / 12 h / Ambient temperature
2: 60 percent / sodium dichromate dihydrate, acetic anhydride / acetic acid / 18 h / Heating
3: 96 percent / lithium aluminum hydride / tetrahydrofuran / 10 h / Heating
4: 86 percent / chromium trioxide / pyridine / 96 h / Ambient temperature
5: 71 percent / sodium cyanoborohydride / methanol / 6 h / pH 7 adjusted with glacial acetic acid
6: 27 percent / polyphosphoric acid / 8 h / 130 °C
With
chromium(VI) oxide; lithium aluminium tetrahydride; aluminium trichloride; PPA; sodium dichromate; acetic anhydride; sodium cyanoborohydride;
In
tetrahydrofuran; pyridine; methanol; acetic acid; nitrobenzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 96 percent / lithium aluminum hydride / tetrahydrofuran / 10 h / Heating
2: 86 percent / chromium trioxide / pyridine / 96 h / Ambient temperature
3: 71 percent / sodium cyanoborohydride / methanol / 6 h / pH 7 adjusted with glacial acetic acid
4: 27 percent / polyphosphoric acid / 8 h / 130 °C
With
chromium(VI) oxide; lithium aluminium tetrahydride; PPA; sodium cyanoborohydride;
In
tetrahydrofuran; pyridine; methanol;
