6-(beta-Bromoethyl)-10,11-methylenedioxy-5,6,7,8-tetrahydrodibenz(c,e)azocine

Base Information

Chemical Name:6-(beta-Bromoethyl)-10,11-methylenedioxy-5,6,7,8-tetrahydrodibenz(c,e)azocine
CAS No.:58532-43-7
Molecular Formula:C18H18BrNO2
Molecular Weight:360.245
Hs Code.:
DSSTox Substance ID:DTXSID50207249
Nikkaji Number:J394.796C
Wikidata:Q83081139
Mol file:58532-43-7.mol

Synonyms:6-(beta-bromoethyl)-10,11-methylenedioxy-5,6,7,8- tetrahydrodibenz(c,e)azocine

Suppliers and Price of 6-(beta-Bromoethyl)-10,11-methylenedioxy-5,6,7,8-tetrahydrodibenz(c,e)azocine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-(beta-Bromoethyl)-10,11-methylenedioxy-5,6,7,8-tetrahydrodibenz(c,e)azocine

Chemical Property:

Vapor Pressure:7.02E-10mmHg at 25°C
Boiling Point:493.5°Cat760mmHg
Flash Point:252.2°C
PSA：21.70000
Density:1.415g/cm³
LogP:3.77320
XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:359.05209
Heavy Atom Count:22
Complexity:380

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CN(CC2=CC=CC=C2C3=CC4=C(C=C31)OCO4)CCBr

Technology Process of 6-(beta-Bromoethyl)-10,11-methylenedioxy-5,6,7,8-tetrahydrodibenz(c,e)azocine

There total 4 articles about 6-(beta-Bromoethyl)-10,11-methylenedioxy-5,6,7,8-tetrahydrodibenz(c,e)azocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58532-42-6
2-(7,8-dihydro-5H-benzo[c][1,3]dioxolo[4',5':4,5]benzo[1,2-e]azocin-6-yl)-ethanol

: 58532-43-7
6-(2-bromo-ethyl)-5,6,7,8-tetrahydro-benzo[c][1,3]dioxolo[4',5':4,5]benzo[1,2-e]azocine

Guidance literature:: With phosphorus tribromide; In benzene;
DOI:10.1248/cpb.25.3312

Reference yield:

: 65762-51-8
2-[6-(2-nitro-vinyl)-benzo[1,3]dioxol-5-yl]-benzoic acid methyl ester

: 58532-43-7
6-(2-bromo-ethyl)-5,6,7,8-tetrahydro-benzo[c][1,3]dioxolo[4',5':4,5]benzo[1,2-e]azocine

Guidance literature:: Multi-step reaction with 3 steps

1: (i) LiAlH₄, Et₂O, (ii) PBr₃, benzene, (iii) EtOH, aq. KOH

2: Et₃N

3: PBr₃ / benzene

With phosphorus tribromide; triethylamine; In benzene;
DOI:10.1248/cpb.25.3312

Reference yield:

: 58532-40-4
5,6,7,8-tetrahydro-benzo[c][1,3]dioxolo[4',5':4,5]benzo[1,2-e]azocine

: 58532-43-7
6-(2-bromo-ethyl)-5,6,7,8-tetrahydro-benzo[c][1,3]dioxolo[4',5':4,5]benzo[1,2-e]azocine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N

2: PBr₃ / benzene

With phosphorus tribromide; triethylamine; In benzene;
DOI:10.1248/cpb.25.3312