5H-Pyrrolo(2,1-c)(1,4)benzodiazepin-5-one, 1,2,3,10,11,11a-hexahydro-

Base Information

Chemical Name:5H-Pyrrolo(2,1-c)(1,4)benzodiazepin-5-one, 1,2,3,10,11,11a-hexahydro-
CAS No.:5544-20-7
Molecular Formula:C₁₂H₁₄N₂O
Molecular Weight:202.256
Hs Code.:
Mol file:5544-20-7.mol

Synonyms:5H-Pyrrolo(2,1-c)(1,4)benzodiazepin-5-one, 1,2,3,10,11,11a-hexahydro-

Suppliers and Price of 5H-Pyrrolo(2,1-c)(1,4)benzodiazepin-5-one, 1,2,3,10,11,11a-hexahydro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 5H-Pyrrolo(2,1-c)(1,4)benzodiazepin-5-one, 1,2,3,10,11,11a-hexahydro-

Chemical Property:

Vapor Pressure:1.05E-06mmHg at 25°C
Boiling Point:403°Cat760mmHg
Flash Point:197.5°C
PSA：32.34000
Density:1.24g/cm³
LogP:1.79260

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5H-Pyrrolo(2,1-c)(1,4)benzodiazepin-5-one, 1,2,3,10,11,11a-hexahydro-

There total 9 articles about 5H-Pyrrolo(2,1-c)(1,4)benzodiazepin-5-one, 1,2,3,10,11,11a-hexahydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 94812-03-0
10-Acetyl-1,2,3,10,11,11a-hexahydro-benzo[e]pyrrolo[1,2-a][1,4]diazepin-5-one

: 5544-20-7
1,2,3,10,11,11a-hexahydro-5H-pyrrolo<2,1-c><1,4>benzodiazepin-5-one

Guidance literature:: With hydrogenchloride; In water; Heating;
DOI:10.1248/cpb.32.3840

Reference yield: 70.0%

: 53160-06-8
N-(2-nitrobenzoyl)pyrrolidine-2-carboxaldehyde

: 5544-20-7
1,2,3,10,11,11a-hexahydro-5H-pyrrolo<2,1-c><1,4>benzodiazepin-5-one

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 4.5h; under 760 Torr;
DOI:10.1021/jo00355a022

Reference yield:

: 11-hydroxy-5-oxo-2,3,11,11a-tetrahydro-1H,5H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-10-carboxylic acid benzyl ester

: 5544-20-7
1,2,3,10,11,11a-hexahydro-5H-pyrrolo<2,1-c><1,4>benzodiazepin-5-one

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; Yield given; Ambient temperature;
DOI:10.1016/S0040-4039(98)02509-X