salvinolone

Base Information

Chemical Name:salvinolone
CAS No.:120278-22-0
Molecular Formula:C₂₀H₂₆O₃
Molecular Weight:314.425
Hs Code.:
Mol file:120278-22-0.mol

Synonyms:9(1H)-Phenanthrenone,2,3,4,4a-tetrahydro-5,6-dihydroxy-1,1,4a-trimethyl-7-(1-methylethyl)-, (S)-;Salvinolone

Suppliers and Price of salvinolone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Arctom
Salvinolone ≥98%
5mg
$ 498.00

Total 8 raw suppliers

Chemical Property of salvinolone

Chemical Property:

PSA：57.53000
LogP:4.81170

Purity/Quality:

99% ^*data from raw suppliers

Salvinolone ≥98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of salvinolone

There total 11 articles about salvinolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.8%

: 337909-73-6
Benzoic acid (4bS,8aS)-4-acetoxy-9-chloro-2-isopropyl-4b,8,8-trimethyl-10-oxo-4b,5,6,7,8,8a,9,10-octahydro-phenanthren-3-yl ester

: 120278-22-0
salvinolone

Guidance literature:: With lithium chloride; In pyridine; for 10h; Heating;
DOI:10.1016/S0968-0896(00)00253-4

Reference yield: 72.5%

: 154842-48-5
11,12-dimethoxyabieta-5,8,11,13-tetraen-7-one

: 120278-22-0
salvinolone

Guidance literature:: With aluminium trichloride; ethanethiol; In dichloromethane; at 3 - 20 ℃; for 4.25h;
DOI:10.1246/bcsj.66.3053

Reference yield:

: 70614-86-7
(4aS,10aS)-7-isopropyl-6-methoxy-1,1,4a-trimethyl-1,2,3,4,4a,10a-hexahydrophenanthrene

: 120278-22-0
salvinolone

Guidance literature:: Multi-step reaction with 7 steps

1: 98.3 percent / H₂ / Pd/C / ethyl acetate / 24 h / 20 °C

2: 94.9 percent / BBr₃ / CH₂Cl₂ / 2 h / 0 - 5 °C

3: 71.4 percent / CHCl₃ / 7 h / 20 °C

4: 76.7 percent / TsOH / toluene / 5 h / Heating

5: 65.9 percent / CrO₃ / acetic acid / 8 h / 20 °C

6: 94.9 percent / SO₂Cl₂ / CCl₄ / 40 h / 60 °C

7: 87.8 percent / LiCl / pyridine / 10 h / Heating

With chromium(VI) oxide; sulfuryl dichloride; hydrogen; boron tribromide; toluene-4-sulfonic acid; lithium chloride; palladium on activated charcoal; In pyridine; tetrachloromethane; dichloromethane; chloroform; acetic acid; ethyl acetate; toluene; 1: hydrogenation / 2: hydrolysis / 3: oxidation; esterification / 4: acetylation / 5: oxidation / 6: chlorination / 7: dehydrohalogenation; hydrolysis;
DOI:10.1016/S0968-0896(00)00253-4