N-[(E)-[(2E)-1,2-bis(4-methoxyphenyl)-2-(phenylhydrazinylidene)ethylidene]amino]aniline

Base Information

• Chemical Name: N-[(E)-[(2E)-1,2-bis(4-methoxyphenyl)-2-(phenylhydrazinylidene)ethylidene]amino]aniline
• CAS No.: 6320-31-6
• Molecular Formula: C₂₈H₂₆N₄O₂
• Molecular Weight: 450.54
• NSC Number: 36867,31781
• Mol file: 6320-31-6.mol

Synonyms:NSC31781;6320-31-6;NSC36867;NSC-31781;NSC-36867;6266-37-1

Chemical Property of N-[(E)-[(2E)-1,2-bis(4-methoxyphenyl)-2-(phenylhydrazinylidene)ethylidene]amino]aniline

Chemical Property:

• Boiling Point: 602.8°Cat760mmHg
• Flash Point: 318.3°C
• Density: 1.12g/cm³
• XLogP3: 7.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 9
• Exact Mass: 450.20557608
• Heavy Atom Count: 34
• Complexity: 583

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)C(=NNC2=CC=CC=C2)C(=NNC3=CC=CC=C3)C4=CC=C(C=C4)OC
• Isomeric SMILES: COC1=CC=C(C=C1)/C(=N\NC2=CC=CC=C2)/C(=N/NC3=CC=CC=C3)/C4=CC=C(C=C4)OC

Technology Process of N-[(E)-[(2E)-1,2-bis(4-methoxyphenyl)-2-(phenylhydrazinylidene)ethylidene]amino]aniline

There total 1 articles about N-[(E)-[(2E)-1,2-bis(4-methoxyphenyl)-2-(phenylhydrazinylidene)ethylidene]amino]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ p-anisil diphenylhydrazone (6266-37-1,6320-31-6,36646-57-8,36646-58-9)

Guidance literature:

Anisaldehyd-phenylhydrazon, akt. MnO2, Bzl., Siedetemp. (neben anderen Verbb.);

DOI:10.1021/jo01282a036

Reference yield: 45.0%

dimethylsilicon dichloride (75-78-5,30107-43-8) + p-anisil diphenylhydrazone (6266-37-1,6320-31-6,36646-57-8,36646-58-9) → 6,7-Bis-(4-methoxy-phenyl)-3,3-dimethyl-2,4-diphenyl-3,4-dihydro-2H-[1,2,4,5,3]tetrazasilepine

Guidance literature:

With pyridine; at -8 - 30 ℃; for 4h;