Copper, dichloro(2-pyridinecarboxaldehyde 2-pyridinylhydrazone)-

Base Information

• Chemical Name: Copper, dichloro(2-pyridinecarboxaldehyde 2-pyridinylhydrazone)-
• CAS No.: 46847-77-2
• Molecular Formula: C11H10Cl2CuN4
• Molecular Weight: 332.6759
• Mol file: 46847-77-2.mol

Synonyms:(pyridine-2-carboxaldehyde-2'-pyridylhydrazonato)copper(II);(pyridine-2-carboxaldehyde-2'-pyridylhydrazonato)Cu(II) dichloride;PCPH-Cu

Chemical Property of Copper, dichloro(2-pyridinecarboxaldehyde 2-pyridinylhydrazone)-

Chemical Property:

• Vapor Pressure: 6.48E-06mmHg at 25°C
• Boiling Point: 378°Cat760mmHg
• Flash Point: 182.4°C
• PSA: 50.17000
• Density: g/cm³
• LogP: -3.99890
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 3
• Exact Mass: 330.957849
• Heavy Atom Count: 18
• Complexity: 205

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=NC(=C1)C=NNC2=CC=CC=N2.[Cl-].[Cl-].[Cu+2]
• Isomeric SMILES: C1=CC=NC(=C1)/C=N/NC2=CC=CC=N2.[Cl-].[Cl-].[Cu+2]

Technology Process of Copper, dichloro(2-pyridinecarboxaldehyde 2-pyridinylhydrazone)-

There total 1 articles about Copper, dichloro(2-pyridinecarboxaldehyde 2-pyridinylhydrazone)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

copper dichloride + 1,3-bis(2′-pyridyl)-1,2-diazapropen-2-ene (2215-33-0) → Cu(2-pyridinecarboxaldehyde 2'-pyridylhydrazone)Cl2 (46847-77-2)

Guidance literature:

In ethanol; addn. of a hot soln. of the ligand in 95% ethanol to a hot soln. of metal(II) salt in ethanol, heated under reflux for 15-30 min; cooled to room temp., filtered off, washed with ethanol and diethyl ether, dried over P2O5 under vac.; elem. anal.;

DOI:10.1016/S0020-1693(00)83485-4

upstream raw materials:

1,3-bis(2′-pyridyl)-1,2-diazapropen-2-ene