perchlorylchloramphenicol

Base Information

Chemical Name:perchlorylchloramphenicol
CAS No.:70487-35-3
Molecular Formula:C₁₁H₁₂Cl₃NO₆
Molecular Weight:360.578
Hs Code.:
Mol file:70487-35-3.mol

Synonyms:Acetamide,2,2-dichloro-N-[2-hydroxy-1-(hydroxymethyl)-2-(4-perchlorylphenyl)ethyl]-,(R*,R*)- (9CI); Acetamide,2,2-dichloro-N-[2-hydroxy-1-(hydroxymethyl)-2-(4-perchlorylphenyl)ethyl]-,(R*,R*)-(?à)-

Suppliers and Price of perchlorylchloramphenicol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of perchlorylchloramphenicol

Chemical Property:

PSA：120.77000
LogP:1.68870

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of perchlorylchloramphenicol

There total 6 articles about perchlorylchloramphenicol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70487-29-5
p-Perchlorylacetophenon

: 70487-35-3
DL-Perchlorylchloramphenicol

Guidance literature:: Multi-step reaction with 7 steps

1: 95 percent / Br₂ / CCl₄ / Heating

2: 1.) hexamethylentetramine; 2.) conc. HCl / 1) heating, 15 min, 2 h, ether, CHCl₃

3: H₂O

4: 70 percent / NaHCO₃ / ethanol; H₂O / 2 h / 35 °C

5: AlCl₃, isopropanol / 1,2-dichloro-ethane / 2 h / Heating

6: 57 percent / 25percent NH₃, Noritcoal / methanol; H₂O / 0.08 h / Heating

7: 2.6 g / NaHCO₃ / methanol / 2 h / Heating

With hydrogenchloride; ammonium hydroxide; aluminium trichloride; hexamethylenetetramine; bromine; sodium hydrogencarbonate; pyrographite; isopropyl alcohol; In methanol; tetrachloromethane; ethanol; water; 1,2-dichloro-ethane;

Reference yield:

: 70487-30-8
p-Perchloryl-α-bromacetophenon

: 70487-35-3
DL-Perchlorylchloramphenicol

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) hexamethylentetramine; 2.) conc. HCl / 1) heating, 15 min, 2 h, ether, CHCl₃

2: H₂O

3: 70 percent / NaHCO₃ / ethanol; H₂O / 2 h / 35 °C

4: AlCl₃, isopropanol / 1,2-dichloro-ethane / 2 h / Heating

5: 57 percent / 25percent NH₃, Noritcoal / methanol; H₂O / 0.08 h / Heating

6: 2.6 g / NaHCO₃ / methanol / 2 h / Heating

With hydrogenchloride; ammonium hydroxide; aluminium trichloride; hexamethylenetetramine; sodium hydrogencarbonate; pyrographite; isopropyl alcohol; In methanol; ethanol; water; 1,2-dichloro-ethane;

Reference yield:

: 70487-32-0
p-Perchloryl-α-acetaminoacetophenon

: 70487-35-3
DL-Perchlorylchloramphenicol

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / NaHCO₃ / ethanol; H₂O / 2 h / 35 °C

2: AlCl₃, isopropanol / 1,2-dichloro-ethane / 2 h / Heating

3: 57 percent / 25percent NH₃, Noritcoal / methanol; H₂O / 0.08 h / Heating

4: 2.6 g / NaHCO₃ / methanol / 2 h / Heating

With ammonium hydroxide; aluminium trichloride; sodium hydrogencarbonate; pyrographite; isopropyl alcohol; In methanol; ethanol; water; 1,2-dichloro-ethane;