2-Propenoic acid,3-[4-(2,3-butadien-1-yloxy)phenyl]-, methyl ester, (2E)-

Base Information

Chemical Name:2-Propenoic acid,3-[4-(2,3-butadien-1-yloxy)phenyl]-, methyl ester, (2E)-
CAS No.:149064-39-1
Molecular Formula:C14H14 O3
Molecular Weight:230.263
Hs Code.:

Synonyms:2-Propenoicacid, 3-[4-(2,3-butadienyloxy)phenyl]-, methyl ester, (2E)- (9CI); 2-Propenoicacid, 3-[4-(2,3-butadienyloxy)phenyl]-, methyl ester, (E)-; Eucalyptene A

Suppliers and Price of 2-Propenoic acid,3-[4-(2,3-butadien-1-yloxy)phenyl]-, methyl ester, (2E)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Propenoic acid,3-[4-(2,3-butadien-1-yloxy)phenyl]-, methyl ester, (2E)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Propenoic acid,3-[4-(2,3-butadien-1-yloxy)phenyl]-, methyl ester, (2E)-

There total 4 articles about 2-Propenoic acid,3-[4-(2,3-butadien-1-yloxy)phenyl]-, methyl ester, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 18668-68-3
4-bromo-buta-1,2-diene

: 3943-97-3
methyl 4-hydroxycinnamate

: 149064-39-1
Eucalyptene A

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1016/j.bmcl.2007.02.084

Reference yield:

: 149068-00-8
4'-(2''-Butynyloxy-4''-chloro)trans-cinnamic acid methyl ester

: 149064-39-1
Eucalyptene A

Guidance literature:: With copper; zinc; In methanol; for 24h; Heating;
DOI:10.1016/S0031-9422(00)95105-7

Reference yield:

: 3943-97-3
methyl 4-hydroxycinnamate

: 149064-39-1
Eucalyptene A

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NaH / 1) THF, 1 h, reflux, 2) THF, 48 h, reflux

2: 95 percent / SOCl₂, pyridine / tetrahydrofuran / 12 h / Heating

3: Cu, Zn / methanol / 24 h / Heating

With pyridine; thionyl chloride; copper; sodium hydride; zinc; In tetrahydrofuran; methanol;
DOI:10.1016/S0031-9422(00)95105-7