b-D-Fructopyranose,2,3-O-(1-methylethylidene)-, cyclic 4,5-sulfate 1-sulfamate

Base Information

• Chemical Name: b-D-Fructopyranose,2,3-O-(1-methylethylidene)-, cyclic 4,5-sulfate 1-sulfamate
• CAS No.: 152191-98-5
• Molecular Formula: C9H15 N O10 S2
• Molecular Weight: 361.351

Synonyms:4H-1,3,2-Dioxathiolo[4,5-d][1,3]dioxolo[4,5-b]pyran,b-D-fructopyranose deriv.; RWJ37947

Chemical Property of b-D-Fructopyranose,2,3-O-(1-methylethylidene)-, cyclic 4,5-sulfate 1-sulfamate

Chemical Property:

Purity/Quality:

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Technology Process of b-D-Fructopyranose,2,3-O-(1-methylethylidene)-, cyclic 4,5-sulfate 1-sulfamate

There total 1 articles about b-D-Fructopyranose,2,3-O-(1-methylethylidene)-, cyclic 4,5-sulfate 1-sulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

Sulfamic acid (3aR,5aS,8aS,8bS)-7,7-dimethyl-2-[(E)-toluene-4-sulfonylimino]-tetrahydro-2λ4-[1,3,2]dioxathiolo[4,5-d][1,3]dioxalo[4,5-b]pyran-5a-ylmethyl ester → Sulfamic acid (2R,3aR,5aS,8aS,8bS)-7,7-dimethyl-2-oxo-2-(toluene-4-sulfonylimino)-tetrahydro-2λ6-[1,3,2]dioxathiolo[4,5-d][1,3]dioxalo[4,5-b]pyran-5a-ylmethyl ester + RWJ-37947 (152191-98-5)

Guidance literature:

With sodium periodate; ruthenium trichloride; In tetrachloromethane; water; acetonitrile; at 5 - 23 ℃; for 20h; Title compound not separated from byproducts;

DOI:10.1021/jm970790w

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