Technology Process of 12-Methylhexadecanoic acid
There total 14 articles about 12-Methylhexadecanoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide; hydrazine hydrate;
In
methanol; diethylene glycol;
125 deg C, 6 h; 195 deg C, 3 h;
- Guidance literature:
-
With
triethylsilane; triethyl aluminum sesquichloride;
In
dichloromethane;
at -15 - 20 ℃;
for 2h;
Title compound not separated from byproducts;
DOI:10.1021/ja048904y
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine / 1 h / 0 °C
2: LiBr / acetone / 5 h / Heating
4: KOH / ethanol; H2O / 5 h / Heating
5: 76 percent / N2H4*H2O, KOH / bis-(2-hydroxy-ethyl) ether; methanol / 125 deg C, 6 h; 195 deg C, 3 h
With
potassium hydroxide; hydrazine hydrate; lithium bromide;
In
pyridine; methanol; ethanol; water; acetone; diethylene glycol;
