(1)Benzopyrano(3,4-b)furo(2,3-h)(1)benzopyran-6(6aH)-one, 12,12a-dihydro-2-isopropyl-8,9-dimethoxy-, (+)-

Base Information

Chemical Name:(1)Benzopyrano(3,4-b)furo(2,3-h)(1)benzopyran-6(6aH)-one, 12,12a-dihydro-2-isopropyl-8,9-dimethoxy-, (+)-
CAS No.:5964-15-8
Molecular Formula:C₂₃H₂₂O₆
Molecular Weight:394.424
Hs Code.:
DSSTox Substance ID:DTXSID10975033

Synonyms:5964-15-8;(1)Benzopyrano(3,4-b)furo(2,3-h)(1)benzopyran-6(6aH)-one, 12,12a-dihydro-2-isopropyl-8,9-dimethoxy-, (+)-;DTXSID10975033;8,9-Dimethoxy-2-(propan-2-yl)-12,12a-dihydrofuro[2',3':7,8][1]benzopyrano[2,3-c][1]benzopyran-6(6aH)-one

Suppliers and Price of (1)Benzopyrano(3,4-b)furo(2,3-h)(1)benzopyran-6(6aH)-one, 12,12a-dihydro-2-isopropyl-8,9-dimethoxy-, (+)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of (1)Benzopyrano(3,4-b)furo(2,3-h)(1)benzopyran-6(6aH)-one, 12,12a-dihydro-2-isopropyl-8,9-dimethoxy-, (+)-

Chemical Property:

Vapor Pressure:2.54E-11mmHg at 25°C
Boiling Point:530.1°Cat760mmHg
Flash Point:274.4°C
Density:1.265g/cm³
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:394.14163842
Heavy Atom Count:29
Complexity:623

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)C1=CC2=C(O1)C=CC3=C2OC4COC5=CC(=C(C=C5C4C3=O)OC)OC

Technology Process of (1)Benzopyrano(3,4-b)furo(2,3-h)(1)benzopyran-6(6aH)-one, 12,12a-dihydro-2-isopropyl-8,9-dimethoxy-, (+)-

There total 22 articles about (1)Benzopyrano(3,4-b)furo(2,3-h)(1)benzopyran-6(6aH)-one, 12,12a-dihydro-2-isopropyl-8,9-dimethoxy-, (+)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 5740-14-7
6a,12a-didehydroisorotenone

: 549-22-4,5964-15-8,6113-82-2,123166-85-8
(+/-)-trans-isorotenone

Guidance literature:: With diisobutylaluminum hydride; In tetrahydrofuran; toluene; at -78 - -20 ℃; for 1h;

Reference yield: 30.0%

: {2-[2-(6-Hydroxy-2-isopropyl-benzofuran-5-yl)-2-oxo-ethyl]-4,5-dimethoxy-phenoxy}-acetaldehyde

: 549-22-4,5964-15-8,6113-82-2,123166-85-8
(+/-)-cis-isorotenone

Guidance literature:: With pyridine; for 0.5h; Heating;

Reference yield:

: 5740-14-7
6a,12a-didehydroisorotenone

: 549-22-4,5964-15-8,6113-82-2,123166-85-8
(+/-)-cis-isorotenone

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / diisoaluminium hydride / tetrahydrofuran / 1 h / -78 °C

2: silica gel plates / hexane; ethyl acetate / 12 h

With diisoaluminium hydride; silica gel; In tetrahydrofuran; hexane; ethyl acetate;