2-METHYL-4-PYRROLIDIN-1-YLANILINE HYDROCHLORIDE

Base Information

• Chemical Name: 2-METHYL-4-PYRROLIDIN-1-YLANILINE HYDROCHLORIDE
• CAS No.: 143525-69-3
• Molecular Formula: C11H16 N2
• Molecular Weight: 176.26
• Hs Code.: 2933990090
• Mol file: 143525-69-3.mol

Synonyms:2-Methyl-4-pyrrolidin-1-ylaniline

Chemical Property of 2-METHYL-4-PYRROLIDIN-1-YLANILINE HYDROCHLORIDE

Chemical Property:

• Vapor Pressure: 2.63E-05mmHg at 25°C
• Boiling Point: 358°Cat760mmHg
• Flash Point: 146.2°C
• PSA: 29.26000
• Density: 1.084g/cm³
• LogP: 2.82360

Purity/Quality:

97% ^*data from raw suppliers

2-Methyl-4-(1-pyrrolidinyl)aniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-METHYL-4-PYRROLIDIN-1-YLANILINE HYDROCHLORIDE

There total 2 articles about 2-METHYL-4-PYRROLIDIN-1-YLANILINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(3-methyl-4-nitro-phenyl)-pyrrolidine (218139-59-4) → 2-methyl-4-pyrrolidino-aniline (143525-69-3)

Guidance literature:

With ethanol; nickel; at 60 ℃; Hydrogenation;

DOI:10.1021/ja01186a070

Reference yield:

4-iodo-2-methyl-1-nitro-benzene (52415-00-6) → 2-methyl-4-pyrrolidino-aniline (143525-69-3)

Guidance literature:

Multi-step reaction with 2 steps

2: Raney nickel; ethanol / 60 °C / Hydrogenation

With ethanol; nickel;

DOI:10.1021/ja01186a070

Reference yield: 56.0%

2-methyl-4-pyrrolidino-aniline (143525-69-3) + 3-butyryl-4-chloro-8-methoxyquinoline (115607-76-6) → 1-[8-Methoxy-4-(2-methyl-4-pyrrolidin-1-yl-phenylamino)-quinolin-3-yl]-butan-1-one

Guidance literature:

In 1,4-dioxane; for 3h; Heating;

DOI:10.1021/jm00014a026

upstream raw materials:

1-(3-methyl-4-nitro-phenyl)-pyrrolidine

4-iodo-2-methyl-1-nitro-benzene

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