(Z)-1-{(5Z)-1-benzyl-5-[(2,2-diethoxyethyl)imino]-1,5-dihydro-4H-imidazol-4-ylidene}-N-ethoxymethanediamine

Base Information

Chemical Name:(Z)-1-{(5Z)-1-benzyl-5-[(2,2-diethoxyethyl)imino]-1,5-dihydro-4H-imidazol-4-ylidene}-N-ethoxymethanediamine
CAS No.:119139-25-2
Molecular Formula:C19H29 N5 O3
Molecular Weight:375.4653
Hs Code.:
Mol file:119139-25-2.mol

Synonyms:NSC 645088

Suppliers and Price of (Z)-1-{(5Z)-1-benzyl-5-[(2,2-diethoxyethyl)imino]-1,5-dihydro-4H-imidazol-4-ylidene}-N-ethoxymethanediamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of (Z)-1-{(5Z)-1-benzyl-5-[(2,2-diethoxyethyl)imino]-1,5-dihydro-4H-imidazol-4-ylidene}-N-ethoxymethanediamine

Chemical Property:

Vapor Pressure:1.03E-07mmHg at 25°C
Boiling Point:433.4°Cat760mmHg
Flash Point:215.9°C
Density:1.17g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (Z)-1-{(5Z)-1-benzyl-5-[(2,2-diethoxyethyl)imino]-1,5-dihydro-4H-imidazol-4-ylidene}-N-ethoxymethanediamine

There total 3 articles about (Z)-1-{(5Z)-1-benzyl-5-[(2,2-diethoxyethyl)imino]-1,5-dihydro-4H-imidazol-4-ylidene}-N-ethoxymethanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 119139-24-1
1-benzyl-5--N'-ethoxy-1H-imidazole-4-carboxamidine

: 119139-25-2
1-benzyl-5-(2,2-diethoxyethylamino)-N'-ethoxy-1H-imidazole-4-carboxamidine

Guidance literature:: With sodium hydroxide; for 3h; Heating;
DOI:10.3987/COM-88-4519

Reference yield:

: 70276-43-6,125661-60-1,125661-61-2
1-Benzyl-N'-ethoxy-5-formamido-1H-imidazole-4-carboxamidine

: 119139-25-2
1-benzyl-5-(2,2-diethoxyethylamino)-N'-ethoxy-1H-imidazole-4-carboxamidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) K₂CO₃, 2.) 18-crown-6 / 1.) DMF, RT, 1 h, 2.) DMF, 30 deg C, 21 h

2: 94 percent / 1N aq. NaOH / 3 h / Heating

With sodium hydroxide; 18-crown-6 ether; potassium carbonate;
DOI:10.1248/cpb.42.1231

Reference yield:

: 51806-20-3
1,1-diethoxy-2-iodoethane

: 119139-25-2
1-benzyl-5-(2,2-diethoxyethylamino)-N'-ethoxy-1H-imidazole-4-carboxamidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) K₂CO₃, 2.) 18-crown-6 / 1.) DMF, RT, 1 h, 2.) DMF, 30 deg C, 21 h

2: 94 percent / 1N aq. NaOH / 3 h / Heating

With sodium hydroxide; 18-crown-6 ether; potassium carbonate;
DOI:10.1248/cpb.42.1231