4-[1-[2-[1-(4-oxo-1-cyclohexa-2,5-dienylidene)ethyl]hydrazinyl]ethylid ene]cyclohexa-2,5-dien-1-one

Base Information

• Chemical Name: 4-[1-[2-[1-(4-oxo-1-cyclohexa-2,5-dienylidene)ethyl]hydrazinyl]ethylid ene]cyclohexa-2,5-dien-1-one
• CAS No.: 5466-24-0
• Molecular Formula: C16H16 N2 O2
• Molecular Weight: 268.315
• Hs Code.: 2928000090
• Mol file: 5466-24-0.mol

Synonyms:Acetophenone,4'-hydroxy-, azine (8CI); Ethanone, 1-(4-hydroxyphenyl)-, [1-(4-hydroxyphenyl)ethylidene]hydrazone(9CI); 4,4'-Dihydroxy-a,a'-dimethylbenzalazine;4-Hydroxyacetophenone azine; NSC 136257; NSC 25771

Chemical Property of 4-[1-[2-[1-(4-oxo-1-cyclohexa-2,5-dienylidene)ethyl]hydrazinyl]ethylid ene]cyclohexa-2,5-dien-1-one

Chemical Property:

• Boiling Point: 374.2°Cat760mmHg
• Flash Point: 130.1°C
• PSA: 58.20000
• Density: 1.225g/cm³
• LogP: 2.80060

Purity/Quality:

99% ^*data from raw suppliers

4,4'-[1,2-hydrazinediylidenebis(1-ethyl-1-ylidene)]diphenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-[1-[2-[1-(4-oxo-1-cyclohexa-2,5-dienylidene)ethyl]hydrazinyl]ethylid ene]cyclohexa-2,5-dien-1-one

There total 3 articles about 4-[1-[2-[1-(4-oxo-1-cyclohexa-2,5-dienylidene)ethyl]hydrazinyl]ethylid ene]cyclohexa-2,5-dien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-Hydroxyacetophenone (99-93-4) → 4,4'dihydroxy-α,α'-dimethylbenzalazine (5466-24-0)

Guidance literature:

With hydrazinium sulfate; In neat (no solvent); at 20 ℃; for 0.133333h;

DOI:10.1016/j.molstruc.2017.05.004

Reference yield:

4-Hydroxyacetophenone (99-93-4) → 4,4'dihydroxy-α,α'-dimethylbenzalazine (5466-24-0)

Guidance literature:

With ethanol; water; sodium carbonate;

Reference yield:

→ 4,4'dihydroxy-α,α'-dimethylbenzalazine (5466-24-0)

Guidance literature:

Aus dem Keton und Hydrazin-Hydrat;

upstream raw materials:

4-Hydroxyacetophenone

Downstream raw materials:

bis(4-butyloxyacetophenon)azine

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