trans,trans-1,3,11-Tridecatriene-5,7,9-triyne

Base Information

• Chemical Name: trans,trans-1,3,11-Tridecatriene-5,7,9-triyne
• CAS No.: 50739-51-0
• Molecular Formula: C13H10
• Molecular Weight: 166.2185
• Nikkaji Number: J2.367.499H,J356.528I,J623.320A
• Mol file: 50739-51-0.mol

Synonyms:1,3,11-Tridecatriene-5,7,9-triyne, (E,E)-;trans,trans-1,3,11-Tridecatriene-5,7,9-triyne;50739-51-0;3-[p-Methoxyphenyl]-4-chloroquinoline;4-Chloro-3-(4-methoxyphenyl)quinoline;1,3(E),11(E)-Tridecatrien-5,7,9-triyne;KAGUESUDHDXNCN-YDFGWWAZSA-N;Trideca-5,7,9-triin-1,3,11-trien;3E,11E-Trideca-1,3,11-triene-5,7,9-triyne;(3E,11E)-1,3,11-Tridecatriene-5,7,9-triyne;(3Z,11E)-1,3,11-Tridecatriene-5,7,9-triyne

Chemical Property of trans,trans-1,3,11-Tridecatriene-5,7,9-triyne

Chemical Property:

• Vapor Pressure: 0.015mmHg at 25°C
• Boiling Point: 265.5°Cat760mmHg
• Flash Point: 105.4°C
• Density: 0.947g/cm³
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 166.078250319
• Heavy Atom Count: 13
• Complexity: 404

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC=CC#CC#CC#CC=CC=C
• Isomeric SMILES: C/C=C/C#CC#CC#C/C=C/C=C

Technology Process of trans,trans-1,3,11-Tridecatriene-5,7,9-triyne

There total 7 articles about trans,trans-1,3,11-Tridecatriene-5,7,9-triyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trideca-1,3c,11ξ-triene-5,7,9-triyne (18668-89-8,50739-51-0,58998-11-1,61434-49-9,124604-44-0) → Trideca-1,3t,11t-trien-5,7,9-triin (50739-51-0)

Guidance literature:

With hydrogenchloride;

Reference yield:

trideca-1,3t,11t-triene-6,9-diyne-5,8-diol (91909-74-9) → trideca-1,3c,11ξ-triene-5,7,9-triyne (18668-89-8,50739-51-0,58998-11-1,61434-49-9,124604-44-0)

Guidance literature:

With thionyl chloride; diethyl ether; Behandeln des Reaktionsprodukts mit aethanol.Kaliumaethylat bei -40grad bis -10grad;

Reference yield:

trideca-1,3t,11t-triene-6,9-diyne-5,8-diol (91909-74-9) → Trideca-1,3t,11t-trien-5,7,9-triin (50739-51-0)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride; diethyl ether / Behandeln des Reaktionsprodukts mit aethanol.Kaliumaethylat bei -40grad bis -10grad

2: iodine / Irradiation_.beim Tageslicht

With thionyl chloride; diethyl ether; iodine;

upstream raw materials:

trideca-1,3t,11t-triene-6,9-diyne-5,8-diol

(E)-penta-2,4-dienal

oct-6t-ene-1,4-diyn-3-ol

trideca-1,3c,11ξ-triene-5,7,9-triyne