4-(4-Bromophenyl)-2-hydroxy-4-oxo-N-tricyclo(3.3.1.1(sup 3,7))dec-1-yl-2-butenamide

Base Information

Chemical Name:4-(4-Bromophenyl)-2-hydroxy-4-oxo-N-tricyclo(3.3.1.1(sup 3,7))dec-1-yl-2-butenamide
CAS No.:126681-80-9
Molecular Formula:C20H22 Br N O3
Molecular Weight:404.2976
Hs Code.:
Wikidata:Q76311391

Synonyms:BRN 4203776;2-Butenamide, 4-(4-bromophenyl)-2-hydroxy-4-oxo-N-tricyclo(3.3.1.1(sup 3,7))dec-1-yl-;4-(4-Bromophenyl)-2-hydroxy-4-oxo-N-tricyclo(3.3.1.1(sup 3,7))dec-1-yl-2-butenamide;126681-80-9;C20-H22-Br-N-O3;LS-46895

Suppliers and Price of 4-(4-Bromophenyl)-2-hydroxy-4-oxo-N-tricyclo(3.3.1.1(sup 3,7))dec-1-yl-2-butenamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4-(4-Bromophenyl)-2-hydroxy-4-oxo-N-tricyclo(3.3.1.1(sup 3,7))dec-1-yl-2-butenamide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.49g/cm³
XLogP3:4.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:403.07831
Heavy Atom Count:25
Complexity:551

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2CC3CC1CC(C2)(C3)NC(=O)C(=O)C=C(C4=CC=C(C=C4)Br)O
Isomeric SMILES:C1C2CC3CC1CC(C2)(C3)NC(=O)C(=O)/C=C(/C4=CC=C(C=C4)Br)\O

Technology Process of 4-(4-Bromophenyl)-2-hydroxy-4-oxo-N-tricyclo(3.3.1.1(sup 3,7))dec-1-yl-2-butenamide

There total 3 articles about 4-(4-Bromophenyl)-2-hydroxy-4-oxo-N-tricyclo(3.3.1.1(sup 3,7))dec-1-yl-2-butenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.8%

: 126681-75-2
2-1-adamantyl)imino>-5-p-bromo-phenyl-2,3-dihydro-3-furanone

: 126681-80-9
4-p-bromo-benzoylpyruvic acid N-(1¹-adamantyl)amide

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; for 3h;
DOI:10.1007/BF00764713

Reference yield:

: 4411-25-0
1-adamantyl isocyanate

: 126681-80-9
4-p-bromo-benzoylpyruvic acid N-(1¹-adamantyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: 68.1 percent / benzene; octane / 1 h / Heating

2: 78.8 percent / 5percent HCl / dioxane / 3 h

With hydrogenchloride; In 1,4-dioxane; octane; benzene;
DOI:10.1007/BF00764713

Reference yield:

: 126681-82-1
5-p-bromo-phenyl-2,3-dihydrofurandione

: 126681-80-9
4-p-bromo-benzoylpyruvic acid N-(1¹-adamantyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: 68.1 percent / benzene; octane / 1 h / Heating

2: 78.8 percent / 5percent HCl / dioxane / 3 h

With hydrogenchloride; In 1,4-dioxane; octane; benzene;
DOI:10.1007/BF00764713