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3,7-Anhydro-1,2-dideoxygluco-oct-2-enitol

Base Information Edit
  • Chemical Name:3,7-Anhydro-1,2-dideoxygluco-oct-2-enitol
  • CAS No.:91797-46-5
  • Molecular Formula:C8H14O5
  • Molecular Weight:190.196
  • Hs Code.:
  • Mol file:91797-46-5.mol
3,7-Anhydro-1,2-dideoxygluco-oct-2-enitol

Synonyms:3,7-anhydro-1,2-dideoxygluco-oct-2-enitol;D-gluco-octenitol

Suppliers and Price of 3,7-Anhydro-1,2-dideoxygluco-oct-2-enitol
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 3 raw suppliers
Chemical Property of 3,7-Anhydro-1,2-dideoxygluco-oct-2-enitol Edit
Chemical Property:
  • Vapor Pressure:5.85E-07mmHg at 25°C 
  • Boiling Point:369.4°Cat760mmHg 
  • Flash Point:177.2°C 
  • PSA:90.15000 
  • Density:1.53g/cm3 
  • LogP:-1.63600 
  • XLogP3:-1.3
  • Hydrogen Bond Donor Count:4
  • Hydrogen Bond Acceptor Count:5
  • Rotatable Bond Count:1
  • Exact Mass:190.08412354
  • Heavy Atom Count:13
  • Complexity:203
Purity/Quality:
Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
  • Canonical SMILES:CC=C1C(C(C(C(O1)CO)O)O)O
  • Isomeric SMILES:C/C=C\1/[C@@H]([C@H]([C@@H]([C@H](O1)CO)O)O)O
Technology Process of 3,7-Anhydro-1,2-dideoxygluco-oct-2-enitol

There total 8 articles about 3,7-Anhydro-1,2-dideoxygluco-oct-2-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium methylate; In methanol; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c3ob41926f
Guidance literature:
Multi-step reaction with 5 steps
1: 1) Mg / 2) ether, 2 h, reflux
2: 53 percent / pyridine / 24 h / Ambient temperature
3: 95 percent / H2 / Pd/C / methanol; ethyl acetate / 5 h
4: 60 percent / pyridine / 18 h / Ambient temperature
5: 1) sodium benzoate, 2) 0.02 N CH3ONa / 1) DMF, 2 h, reflux, 2) 12 h, room temp.
With pyridine; sodium benzoate; hydrogen; sodium methylate; magnesium; palladium on activated charcoal; In methanol; ethyl acetate;
Guidance literature:
Multi-step reaction with 7 steps
1: 1) 0.02N NaOCH3, 2) NaH / 1) 3.5 h, 2) DMF, 12 h, r.t.
2: 89 percent / p-TsOH*H2O / CH2Cl2; acetone / 2 h
3: 1) Mg / 2) ether, 2 h, reflux
4: 53 percent / pyridine / 24 h / Ambient temperature
5: 95 percent / H2 / Pd/C / methanol; ethyl acetate / 5 h
6: 60 percent / pyridine / 18 h / Ambient temperature
7: 1) sodium benzoate, 2) 0.02 N CH3ONa / 1) DMF, 2 h, reflux, 2) 12 h, room temp.
With pyridine; sodium benzoate; hydrogen; sodium methylate; sodium hydride; toluene-4-sulfonic acid; magnesium; palladium on activated charcoal; In methanol; dichloromethane; ethyl acetate; acetone;
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