Germacyclopentane

Base Information

Chemical Name:Germacyclopentane
CAS No.:3466-01-1
Molecular Formula:C4H10Ge
Molecular Weight:0
Hs Code.:
Mol file:3466-01-1.mol

Synonyms:Germacyclopentan;Germano-cyclopentan;Germanocyclopentan;Germolane;Silacyclopentan;Germacyclopentane;

Suppliers and Price of Germacyclopentane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of Germacyclopentane

Chemical Property:

Boiling Point:91 - 92 °C (760 mmHg)
PSA：0.00000
LogP:1.54600

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Germacyclopentane

There total 3 articles about Germacyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-52-1
1,4-dibromo-butane

: 10038-98-9
germaniumtetrachloride

: 3466-01-1
Germacyclopentan

Guidance literature:: With magnesium; In diethyl ether; under N2; C4H8Br2 in anhyd. Et2O added to Mg turnings; added dropwise toGeCl4 in Et2O with stirring over 1 h; refluxed for 6 h; cooled to room temp.; stirred for 20 h; filtered; ppt. washed with dry ether; ether removed by distn. under vac.at 30°C and then at 80°C; purified by low temp., low pres sure fractionation column; detd. by NMR and IR spectra;
DOI:10.1016/j.molstruc.2006.11.050

Reference yield:

: 16853-85-3
lithium aluminium tetrahydride

: 10038-98-9
germaniumtetrachloride

: 23708-47-6
1,4-bis(bromomagnesium)butane

: 3466-01-1
Germacyclopentan

Guidance literature:: In not given; according to P. Mazerolles, Bull. Soc. Chem. Fr., 1962, 1907;
DOI:10.1246/bcsj.64.91

Reference yield:

: 3466-01-1
Germacyclopentan

Guidance literature:: GeCl4, 1) Ether, ether. BrMg(CH2)4MgBr, 2) LiAlH4, sd.Ether (Red.) (Ausb.18.6percent, auf GeCl4 ber.) (neben 5-Germano-spiro<4.4>nonan und anderen Produkten);

upstream raw materials:

lithium aluminium tetrahydride

germaniumtetrachloride

1,4-bis(bromomagnesium)butane

1,4-dibromo-butane

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