4-methylphenyl dichloroacetate

Base Information

Chemical Name:4-methylphenyl dichloroacetate
CAS No.:18133-58-9
Molecular Formula:C9H8 Cl2 O2
Molecular Weight:219.067
Hs Code.:

Synonyms:Aceticacid, dichloro-, 4-methylphenyl ester (9CI); Aceticacid, dichloro-, p-tolylester (8CI); NSC 55408

Suppliers and Price of 4-methylphenyl dichloroacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4-methylphenyl dichloroacetate

Chemical Property:

Vapor Pressure:0.00932mmHg at 25°C
Boiling Point:265.1°Cat760mmHg
Flash Point:107.3°C
Density:1.315g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-methylphenyl dichloroacetate

There total 5 articles about 4-methylphenyl dichloroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 15081-00-2
p-methylphenyl trichloroacetate

: 18133-58-9
4-methylphenyl dichloroacetate

: C₁₈H₁₄Cl₂O₄

Guidance literature:: With [2,2]bipyridinyl; copper(l) chloride; In benzene; for 2h; Solvent; stereoselective reaction; Schlenk technique; Inert atmosphere; Reflux; Cooling with ice;
DOI:10.1016/j.molstruc.2019.02.018

Reference yield:

: 79-36-7
dichloroacethyl chloride

: 106-44-5
p-cresol

: 18133-58-9
4-methylphenyl dichloroacetate

Guidance literature:: With pyridine; In diethyl ether; at 20 ℃;
DOI:10.1039/a900189a

Reference yield:

: 106-44-5
p-cresol

: 18133-58-9
4-methylphenyl dichloroacetate

: C₁₈H₁₄Cl₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / diethyl ether / 0 - 5 °C

2: copper(l) chloride; [2,2]bipyridinyl / benzene / 2 h / Schlenk technique; Inert atmosphere; Reflux; Cooling with ice

With [2,2]bipyridinyl; triethylamine; copper(l) chloride; In diethyl ether; benzene;
DOI:10.1016/j.molstruc.2019.02.018