s-Naphthalen-2-yl 4-nitrobenzenecarbothioate

Base Information

Chemical Name:s-Naphthalen-2-yl 4-nitrobenzenecarbothioate
CAS No.:6629-65-8
Molecular Formula:C17H11NO3S
Molecular Weight:309.345
Hs Code.:
NSC Number:57979
DSSTox Substance ID:DTXSID60288887
Nikkaji Number:J2.105.273F
Wikidata:Q82026022

Synonyms:6629-65-8;s-naphthalen-2-yl 4-nitrobenzenecarbothioate;NSC57979;NCIOpen2_007670;DTXSID60288887;NSC-57979

Suppliers and Price of s-Naphthalen-2-yl 4-nitrobenzenecarbothioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of s-Naphthalen-2-yl 4-nitrobenzenecarbothioate

Chemical Property:

Vapor Pressure:3.49E-10mmHg at 25°C
Boiling Point:501.4°Cat760mmHg
Flash Point:257°C
Density:1.38g/cm³
XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:309.04596439
Heavy Atom Count:22
Complexity:415

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C=C(C=CC2=C1)SC(=O)C3=CC=C(C=C3)[N+](=O)[O-]

Technology Process of s-Naphthalen-2-yl 4-nitrobenzenecarbothioate

There total 4 articles about s-Naphthalen-2-yl 4-nitrobenzenecarbothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 91-60-1
2-Naphthalenethiol

: 62-23-7
4-nitro-benzoic acid

: 6629-65-8
S-2-naphthyl 4-nitrobenzenecarbothioate

Guidance literature:: With Methanesulfonic anhydride; at 80 ℃; for 4h;
DOI:10.1007/s12039-020-01871-5

Reference yield:

: 403-50-9
p-nitrobenzoyl fluoride

: 91-60-1
2-Naphthalenethiol

: 6629-65-8
S-2-naphthyl 4-nitrobenzenecarbothioate

Guidance literature:: With dmap; In dichloromethane; at 20 ℃;
DOI:10.1055/s-2004-831250

Reference yield:

: 62-23-7
4-nitro-benzoic acid

: 6629-65-8
S-2-naphthyl 4-nitrobenzenecarbothioate

Guidance literature:: Multi-step reaction with 2 steps

1: tetramethylfluoroformamidinium hexafluorophosphate; Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

2: 0.70 g / DMAP / CH₂Cl₂ / 20 °C

With dmap; triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; In dichloromethane;
DOI:10.1055/s-2004-831250