2-Nitrosomethylaminopyridine

Base Information

• Chemical Name: 2-Nitrosomethylaminopyridine
• CAS No.: 16219-98-0
• Molecular Formula: C6H7 N3 O
• Molecular Weight: 137.141
• UNII: 739F0M5S0H
• DSSTox Substance ID: DTXSID4021050
• Nikkaji Number: J35.410D
• Wikidata: Q27266163
• ChEMBL ID: CHEMBL165013
• Mol file: 16219-98-0.mol

Synonyms:2-nitrosomethylaminopyridine;N-nitroso-N-methyl-2-aminopyridine

Chemical Property of 2-Nitrosomethylaminopyridine

Chemical Property:

• Vapor Pressure: 0.00262mmHg at 25°C
• Boiling Point: 286.6°Cat760mmHg
• Flash Point: 127.1°C
• Density: 1.17g/cm³
• XLogP3: 1.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 1
• Exact Mass: 137.058911855
• Heavy Atom Count: 10
• Complexity: 118

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C1=CC=CC=N1)N=O

Technology Process of 2-Nitrosomethylaminopyridine

There total 3 articles about 2-Nitrosomethylaminopyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-(N-methylamino)pyridine (4597-87-9) → N-methyl-N-(pyridin-2-yl)nitrous amide (16219-98-0)

Guidance literature:

With hydrogenchloride; sodium nitrite;

Reference yield: 30.0%

2-(Dimethylamino)pyridine (5683-33-0) → N-methyl-N-(pyridin-2-yl)nitrous amide (16219-98-0)

Guidance literature:

With tert.-butylnitrite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In acetonitrile; at 45 ℃; for 10h;

DOI:10.1039/c7gc02775c

Reference yield:

→ N-methyl-N-(pyridin-2-yl)nitrous amide (16219-98-0)

Guidance literature:

2-Methylamino-pyridin in wss. HCl, wss. Na-Nitrit, 5grad;

DOI:10.1039/j29670000273

upstream raw materials:

2-(N-methylamino)pyridine

2-(Dimethylamino)pyridine

Downstream raw materials:

N-methyl-N-(pyridin-2-yl)hydrazine

Methyl-pyridin-2-yl-carbamic acid ethyl ester

4-nitro-benzaldehyde-(methyl-[2]pyridyl-hydrazone)

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