D-Galactose,2-amino-3-O-[(1R)-1-carboxyethyl]-2-deoxy-

Base Information

Chemical Name:D-Galactose,2-amino-3-O-[(1R)-1-carboxyethyl]-2-deoxy-
CAS No.:24874-28-0
Molecular Formula:C₉H₁₇NO₇
Molecular Weight:251.236
Hs Code.:
Mol file:24874-28-0.mol

Synonyms:Galactopyranose,2-amino-3-O-(D-1-carboxyethyl)-2-deoxy-, D- (8CI);2-Amino-3-O-(D-1-carboxyethyl)-2-deoxy-D-galactopyranose; D-Galactomuramicacid; Galactomuramic acid

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Chemical Property of D-Galactose,2-amino-3-O-[(1R)-1-carboxyethyl]-2-deoxy-

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Technology Process of D-Galactose,2-amino-3-O-[(1R)-1-carboxyethyl]-2-deoxy-

There total 9 articles about D-Galactose,2-amino-3-O-[(1R)-1-carboxyethyl]-2-deoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40642-89-5
2-((4aR,6S,7R,8R,8aS)-7-Acetylamino-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionic acid

: 484-57-1,14599-65-6,24874-28-0,40461-66-3,40525-29-9,41546-27-4,41546-28-5
isomuramic acid

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; diethyl ether

2: 1) HCl, 2) Dowex 1-X₄ (OH^-) resin / 1) H₂O, reflux, 4 h, 2) H₂O, pH 6

With hydrogenchloride; Dowex 1-X₄ (OH^-) resin; In methanol; diethyl ether;
DOI:10.1016/S0008-6215(96)00271-6

Reference yield:

: 6619-04-1
N-((4aR,6S,7R,8R,8aS)-8-Hydroxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-acetamide

: 484-57-1,14599-65-6,24874-28-0,40461-66-3,40525-29-9,41546-27-4,41546-28-5
isomuramic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NaH, 2) NaOH / 1) THF, reflux, 2 h; room temperature, overnight, 2) MeOH, H₂O, 50 deg C, 30 min

2: methanol; diethyl ether

3: 1) HCl, 2) Dowex 1-X₄ (OH^-) resin / 1) H₂O, reflux, 4 h, 2) H₂O, pH 6

With hydrogenchloride; sodium hydroxide; Dowex 1-X₄ (OH^-) resin; sodium hydride; In methanol; diethyl ether;
DOI:10.1016/S0008-6215(96)00271-6