2,4-Oxazolidinedione,5-[[2-[(5-methyl-2- phenyl-4-oxazolyl)methyl]-5-benzofuranyl]- methyl]-

Base Information

Chemical Name:2,4-Oxazolidinedione,5-[[2-[(5-methyl-2- phenyl-4-oxazolyl)methyl]-5-benzofuranyl]- methyl]-
CAS No.:132646-45-8
Molecular Formula:C₂₃H₁₈N₂O₅
Molecular Weight:402.406
Hs Code.:

Synonyms:

Suppliers and Price of 2,4-Oxazolidinedione,5-[[2-[(5-methyl-2- phenyl-4-oxazolyl)methyl]-5-benzofuranyl]- methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,4-Oxazolidinedione,5-[[2-[(5-methyl-2- phenyl-4-oxazolyl)methyl]-5-benzofuranyl]- methyl]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,4-Oxazolidinedione,5-[[2-[(5-methyl-2- phenyl-4-oxazolyl)methyl]-5-benzofuranyl]- methyl]-

There total 10 articles about 2,4-Oxazolidinedione,5-[[2-[(5-methyl-2- phenyl-4-oxazolyl)methyl]-5-benzofuranyl]- methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 132646-44-7
5-<2-<<(5-methyl-2-phenyl-4-oxazolyl)methyl>-5-benzofuranyl>methylidene>-2,4-oxazolidinedione

: 132646-45-8
5-(2-(5-methyl-2-phenyloxazol-4-ylmethyl)-benzofuran-5-ylmethyl)-oxazolidine-2,4-dione

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; under 2068.6 Torr; Ambient temperature;
DOI:10.1021/jm00109a003

Reference yield:

: 103788-62-1
4-bromoacetyl-5-methyl-2-phenyl-oxazole

: 132646-45-8
5-(2-(5-methyl-2-phenyloxazol-4-ylmethyl)-benzofuran-5-ylmethyl)-oxazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 8 steps

1: 53 percent / NaOCH₃ / ethanol / Heating

2: 90 percent / NaBH₄ / tetrahydrofuran; methanol / 1 h / Ambient temperature

3: 100 percent / CF₃COOH, triethylsilane / 1 h / 0 °C

4: 58 percent / dimethylformamide / 18 h / 150 °C

5: 87 percent / Ni-Al alloy, 70percent aq. HCOOH / 2 h / Heating

6: 73 percent / anhyd. sodium acetate / 1.5 h / 120 °C / 0.1 Torr

7: 66 percent / m-chloroperbenzoic acid / dimethylformamide / 2.5 h / Ambient temperature

8: 68 percent / H₂ / 10percent Pd/C / tetrahydrofuran / 2068.6 Torr / Ambient temperature

With triethylsilane; sodium tetrahydroborate; formic acid; aluminum nickel; hydrogen; sodium methylate; sodium acetate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00109a003

Reference yield:

: 1761-61-1
5-bromosalicyclaldehyde

: 132646-45-8
5-(2-(5-methyl-2-phenyloxazol-4-ylmethyl)-benzofuran-5-ylmethyl)-oxazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 8 steps

1: 53 percent / NaOCH₃ / ethanol / Heating

2: 90 percent / NaBH₄ / tetrahydrofuran; methanol / 1 h / Ambient temperature

3: 100 percent / CF₃COOH, triethylsilane / 1 h / 0 °C

4: 58 percent / dimethylformamide / 18 h / 150 °C

5: 87 percent / Ni-Al alloy, 70percent aq. HCOOH / 2 h / Heating

6: 73 percent / anhyd. sodium acetate / 1.5 h / 120 °C / 0.1 Torr

7: 66 percent / m-chloroperbenzoic acid / dimethylformamide / 2.5 h / Ambient temperature

8: 68 percent / H₂ / 10percent Pd/C / tetrahydrofuran / 2068.6 Torr / Ambient temperature

With triethylsilane; sodium tetrahydroborate; formic acid; aluminum nickel; hydrogen; sodium methylate; sodium acetate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00109a003