1a,9b-Dihydro-1H-phenanthro(9,10-b)azirine

Base Information

Chemical Name:1a,9b-Dihydro-1H-phenanthro(9,10-b)azirine
CAS No.:67464-46-4
Molecular Formula:C14H11N
Molecular Weight:193.248
Hs Code.:
NSC Number:352297,305486
DSSTox Substance ID:DTXSID10986740

Synonyms:phenanthrene 9,10-imine

Suppliers and Price of 1a,9b-Dihydro-1H-phenanthro(9,10-b)azirine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
PHENANTHRENE-9,10-IMINE 95.00%
5MG
$ 505.92

Total 4 raw suppliers

Chemical Property of 1a,9b-Dihydro-1H-phenanthro(9,10-b)azirine

Chemical Property:

Vapor Pressure:7E-05mmHg at 25°C
Boiling Point:343.5°Cat760mmHg
Flash Point:175.4°C
PSA：21.94000
Density:1.201g/cm³
LogP:3.38140
XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:193.089149355
Heavy Atom Count:15
Complexity:236

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

PHENANTHRENE-9,10-IMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3C(N3)C4=CC=CC=C42

Technology Process of 1a,9b-Dihydro-1H-phenanthro(9,10-b)azirine

There total 9 articles about 1a,9b-Dihydro-1H-phenanthro(9,10-b)azirine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 53581-32-1
(+/-)-trans-9-Azido-10-hydroxy-9,10-dihydrophenanthrene

: 67464-46-4
1a,9b-dihydro-1H-phenanthro<9,10-b>azirine

Guidance literature:: With phosphorous acid trimethyl ester; In dichloromethane; for 3h; Heating;

Reference yield: 17.0%

: 316-31-4
5H-dibenzazepine

: 67464-46-4
1a,9b-dihydro-1H-phenanthro<9,10-b>azirine

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; 1.) -78 deg C, 3 h, 2.) 50 deg C, 48 h;
DOI:10.1021/jo00380a010