Bicyclo(3.3.1)non-1-ene

Base Information

Chemical Name:Bicyclo(3.3.1)non-1-ene
CAS No.:17530-61-9
Molecular Formula:C₉H₁₄
Molecular Weight:122.21
Hs Code.:
DSSTox Substance ID:DTXSID10938648

Synonyms:Bicyclo(3.3.1)non-1-ene;17530-61-9;Bicyclo[3.3.1]non-1-ene;bicyclo[3.3.1]nonene;DTXSID10938648

Suppliers and Price of Bicyclo(3.3.1)non-1-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Bicyclo(3.3.1)non-1-ene

Chemical Property:

Vapor Pressure:1.19mmHg at 25°C
Boiling Point:180.9°Cat760mmHg
Flash Point:42.4°C
PSA：0.00000
Density:0.91g/cm³
LogP:2.89680
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:122.109550447
Heavy Atom Count:9
Complexity:133

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC2CCC=C(C1)C2

Technology Process of Bicyclo(3.3.1)non-1-ene

There total 20 articles about Bicyclo(3.3.1)non-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(η2-1-bicyclo{3.3.1}nonene)dicarbonyl(η5-cyclopentadienyl)iron(II) tetrafluoroborate: (η2-1-bicyclo{3.3.1}nonene)dicarbonyl(η5-cyclopentadienyl)iron(II) tetrafluoroborate

: 1184-78-7
trimethylamine-N-oxide

: 17530-61-9,54674-58-7,82509-63-5
(Z)-bicyclo{3.3.1}non-1-ene

Guidance literature:: In dichloromethane; react. of (C9H14)Fe(CO)2(C5H5)BF4 with anhyd. trimethylamine oxide at -20°C; identified by NMR;
DOI:10.1021/ja00231a023

Reference yield:

: 26775-58-6
3-(3,3-Diaethoxycarbonyl-cyclohexen-1-yl-1)-propen-2-saeureaethylester

: 17530-61-9,54674-58-7,82509-63-5
bicyclo[3.3.1]non-1-ene

Guidance literature:: Multi-step reaction with 10 steps

1: H₂ / PtO₂ / ethanol

2: NaH / 1,2-dimethoxy-ethane

3: aq. KOH / methanol

4: H₂SO₄ / 1,2-dichloro-ethane

5: Al(OiPr)3

6: aq. KOH / ethanol

7: diethyl ether

8: Py

9: aq. KOH, Py / ethanol

10: KOtBu / dimethylsulfoxide

With pyridine; potassium hydroxide; sulfuric acid; potassium tert-butylate; hydrogen; aluminum isopropoxide; sodium hydride; platinum(IV) oxide; In methanol; 1,2-dimethoxyethane; diethyl ether; ethanol; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1021/ja00707a034

Reference yield:

: 26775-57-5
3-formyl-cyclohex-3-ene-1,1-dicarboxylic acid diethyl ester

: 17530-61-9,54674-58-7,82509-63-5
bicyclo[3.3.1]non-1-ene

Guidance literature:: Multi-step reaction with 11 steps

1: NaH / 1,2-dimethoxy-ethane

2: H₂ / PtO₂ / ethanol

3: NaH / 1,2-dimethoxy-ethane

4: aq. KOH / methanol

5: H₂SO₄ / 1,2-dichloro-ethane

6: Al(OiPr)3

7: aq. KOH / ethanol

8: diethyl ether

9: Py

10: aq. KOH, Py / ethanol

11: KOtBu / dimethylsulfoxide

With pyridine; potassium hydroxide; sulfuric acid; potassium tert-butylate; hydrogen; aluminum isopropoxide; sodium hydride; platinum(IV) oxide; In methanol; 1,2-dimethoxyethane; diethyl ether; ethanol; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1021/ja00707a034