Bis(5-nitropyridin-2-yl)sulfane

Base Information

• Chemical Name: Bis(5-nitropyridin-2-yl)sulfane
• CAS No.: 2127-11-9
• Molecular Formula: C10H6N4O4S
• Molecular Weight: 278.244
• Mol file: 2127-11-9.mol

Synonyms:

Chemical Property of Bis(5-nitropyridin-2-yl)sulfane

Chemical Property:

• Boiling Point: 539.4°Cat760mmHg
• Flash Point: 280°C
• Density: 1.6g/cm³

Purity/Quality:

99%min ^*data from raw suppliers

5-Nitro-2-[(5-nitropyridin-2-yl)sulfanyl]pyridine 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bis(5-nitropyridin-2-yl)sulfane

There total 8 articles about Bis(5-nitropyridin-2-yl)sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-5-nitropyridine (4548-45-2) → Bis-<5-nitro-pyridyl-(2)>-sulfid (2127-11-9)

Guidance literature:

With sodium sulfide; ethanol; water;

DOI:10.1021/ja01858a051

Reference yield:

2-chloro-5-nitropyridine (4548-45-2) + thiourea (17356-08-0) → Bis-<5-nitro-pyridyl-(2)>-sulfid (2127-11-9)

Guidance literature:

With water;

DOI:10.1021/ja01864a017

Reference yield:

2-chloro-5-nitropyridine (4548-45-2) → Bis-<5-nitro-pyridyl-(2)>-sulfid (2127-11-9)

Guidance literature:

With ethylene glycol; at 180 ℃;

upstream raw materials:

2-chloro-5-nitropyridine

2-mercapto-5-nitropyridine

thiourea

water

Downstream raw materials:

6,6'-sulfanediyl-bis-pyridin-3-ylamine

Refernces

• 1、 Davydov,Beletskaya. "Synthesis of diaryl sulfides by the reactions of activated aryl halides with potassium ethyl dithiocarbonate under conditions of phase-transfer catalysis [2]". . p. 278 - 278. Retrieved 2007/10/03.