1,3,4,6-tetra-O-acetyl-2-[acetyl(methyl)amino]-2-deoxyhexopyranose

Base Information

• Chemical Name: 1,3,4,6-tetra-O-acetyl-2-[acetyl(methyl)amino]-2-deoxyhexopyranose
• CAS No.: 7460-96-0
• Molecular Formula: C₁₇H₂₅NO₁₀
• Molecular Weight: 403.386
• Mol file: 7460-96-0.mol

Synonyms:

Chemical Property of 1,3,4,6-tetra-O-acetyl-2-[acetyl(methyl)amino]-2-deoxyhexopyranose

Chemical Property:

• Vapor Pressure: 3.5E-10mmHg at 25°C
• Boiling Point: 501.3°C at 760 mmHg
• Flash Point: 257°C
• Density: 1.28g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3,4,6-tetra-O-acetyl-2-[acetyl(methyl)amino]-2-deoxyhexopyranose

There total 7 articles about 1,3,4,6-tetra-O-acetyl-2-[acetyl(methyl)amino]-2-deoxyhexopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ N-Methyl-2-acetamido-2-deoxy-1,3,4,6-tetra-O-acetyl-L-glucopyranose (7460-96-0)

Guidance literature:

With sodium hydroxide; dimethyl sulfate; Behandeln des Reaktionsprodukts mit Acetanhydrid und Pyridin und Erhitzen des danach isolierten Reaktionsprodukts mit Zinkchlorid und Acetanhydrid;

DOI:10.1021/ja01204a029

Reference yield:

→ N-Methyl-2-acetamido-2-deoxy-1,3,4,6-tetra-O-acetyl-L-glucopyranose (7460-96-0)

Guidance literature:

With hydrogenchloride; sodium amalgam; Behandeln des Reaktionsprodukts mit Acetanhydrid und Pyridin;

DOI:10.1021/ja01204a029

Reference yield:

→ N-Methyl-2-acetamido-2-deoxy-1,3,4,6-tetra-O-acetyl-L-glucopyranose (7460-96-0) + N-Methyl-pentaacetyl-α-L-glucosamin (7460-96-0,23590-90-1,40983-15-1)

Guidance literature:

With pyridine; acetic anhydride;

DOI:10.1021/ja01203a050 DOI:10.1021/ja01200a002

upstream raw materials:

tetra-O-acetyl-2-(acetyl-methyl-amino)-2-deoxy-α-D-glucopyranose

Downstream raw materials:

tetra-O-acetyl-2-(acetyl-methyl-amino)-2-deoxy-α-DL-glucopyranose