methyl 6-[(2S,3R,4S,5R)-3,4,5-trihydroxy-2-methylpiperidin-1-yl]hexanoate

Base Information

Chemical Name:methyl 6-[(2S,3R,4S,5R)-3,4,5-trihydroxy-2-methylpiperidin-1-yl]hexanoate
CAS No.:116265-56-6
Molecular Formula:C₁₃H₂₅NO₅
Molecular Weight:275.345
Hs Code.:

Synonyms:1-Piperidinehexanoicacid, 3,4,5-trihydroxy-2-methyl-, methyl ester, [2S-(2a,3a,4a,5b)]-;1,5-Dideoxy-1,5-imino-N-[5-(methoxycarbonyl)pentyl]-L-fucitol

Suppliers and Price of methyl 6-[(2S,3R,4S,5R)-3,4,5-trihydroxy-2-methylpiperidin-1-yl]hexanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 6-[(2S,3R,4S,5R)-3,4,5-trihydroxy-2-methylpiperidin-1-yl]hexanoate

Chemical Property:

Vapor Pressure:6.33E-09mmHg at 25°C
Boiling Point:422.9°Cat760mmHg
Flash Point:209.6°C
Density:1.186g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl 6-[(2S,3R,4S,5R)-3,4,5-trihydroxy-2-methylpiperidin-1-yl]hexanoate

There total 7 articles about methyl 6-[(2S,3R,4S,5R)-3,4,5-trihydroxy-2-methylpiperidin-1-yl]hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 6654-36-0
methyl 6-oxohexanoate

: 99212-30-3,449729-69-5,528593-83-1
deoxyfuconojirimycin

: 116265-56-6
1,5-Didesoxy-1,5-imino-N-<5-(methoxycarbonyl)pentyl>-L-fucit

Guidance literature:: With water; hydrogen; acetic acid; palladium dihydroxide; In methanol; for 12h; under 7500.6 Torr;

Reference yield:

: 68733-26-6
2-deoxy-2-azidogalactopyranose

: 116265-56-6
1,5-Didesoxy-1,5-imino-N-<5-(methoxycarbonyl)pentyl>-L-fucit

Guidance literature:: Multi-step reaction with 8 steps

1: 72 percent / 6M HCl / 22 h / Ambient temperature

2: 59 percent / pyridine / 2 h / 70 °C

3: pyridine / 1 h / Ambient temperature

4: 1.) formic acid 2.) pyridine / 1.) Et₂O, 2.) 5 deg C, 14 h

5: 61 percent / H₂O, triphenylphosphine / CHCl₃ / 7 h / Ambient temperature

6: 87 percent / H₂ / Raney-nickel / ethyl acetate; ethanol / 7 h / Heating

7: 97 percent / NH₃/MeOH / 12 h / Ambient temperature

8: 95 percent / H₂O, CH₃COOH, H₂ / Pd(OH)2/C / methanol / 12 h / 7500.6 Torr

With pyridine; hydrogenchloride; methanol; formic acid; ammonia; water; hydrogen; acetic acid; triphenylphosphine; palladium dihydroxide; nickel; In pyridine; methanol; ethanol; chloroform; ethyl acetate;

Reference yield:

: 116265-41-9
2-Azido-2-desoxy-D-galactose-trimethylendithioacetal

: 116265-56-6
1,5-Didesoxy-1,5-imino-N-<5-(methoxycarbonyl)pentyl>-L-fucit

Guidance literature:: Multi-step reaction with 7 steps

1: 59 percent / pyridine / 2 h / 70 °C

2: pyridine / 1 h / Ambient temperature

3: 1.) formic acid 2.) pyridine / 1.) Et₂O, 2.) 5 deg C, 14 h

4: 61 percent / H₂O, triphenylphosphine / CHCl₃ / 7 h / Ambient temperature

5: 87 percent / H₂ / Raney-nickel / ethyl acetate; ethanol / 7 h / Heating

6: 97 percent / NH₃/MeOH / 12 h / Ambient temperature

7: 95 percent / H₂O, CH₃COOH, H₂ / Pd(OH)2/C / methanol / 12 h / 7500.6 Torr

With pyridine; methanol; formic acid; ammonia; water; hydrogen; acetic acid; triphenylphosphine; palladium dihydroxide; nickel; In pyridine; methanol; ethanol; chloroform; ethyl acetate;