2,4-Bis(1-methyl-1-phenylethyl)-6-((2-nitrophenyl)azo)phenol

Base Information

Chemical Name:2,4-Bis(1-methyl-1-phenylethyl)-6-((2-nitrophenyl)azo)phenol
CAS No.:70693-50-4
Deprecated CAS:1098589-90-2
Molecular Formula:C₃₀H₂₉N₃O₃
Molecular Weight:479.579
Hs Code.:
European Community (EC) Number:274-768-2
UNII:L27V2914MR
DSSTox Substance ID:DTXSID1028994
Nikkaji Number:J288.768A
Wikidata:Q27282611
Mol file:70693-50-4.mol

Synonyms:2,4-Bis(1-methyl-1-phenylethyl)-6-((2-nitrophenyl)azo)phenol;70693-50-4;EINECS 274-768-2;UNII-L27V2914MR;L27V2914MR;Phenol, 2,4-bis(1-methyl-1-phenylethyl)-6-((2-nitrophenyl)azo)-;2-Nitro-2'-hydroxy-3',5'-bis(alpha,alpha-dimethylbenzyl)azobenzene;Phenol, 2,4-bis(1-methyl-1-phenylethyl)-6-(2-(2-nitrophenyl)diazenyl)-;C30H29N3O3;2,4-BIS(1-METHYL-1-PHENYLETHYL)-6-[(2-NITROPHENYL)AZO]PHENOL;Phenol, 2,4-bis(1-methyl-1-phenylethyl)-6-[(2-nitrophenyl)azo]-;C30-H29-N3-O3;Phenol, 2,4-bis(1-methyl-1-phenylethyl)-6-[2-(2-nitrophenyl)diazenyl]-;SCHEMBL6860824;DTXSID1028994;LS-195673;Q27282611;2,4-bis-(1-Methyl-1-phenylethyl)-6-[(2-nitrophenyl)azo]phenol;2-Nitro-2'-hydroxy-3',5'-di(alpha,alpha-dimethylbenzyl)azobenzene;2-nitro-2'-hydroxy-3',5'-di-(alpha,alpha-dimethylbenzyl)azobenzene;2,4-bis(1-methyl-1-phenylethyl)-6-[(E)-(2-nitrophenyl)diazenyl]phenol;2-nitro-2'-hydroxy-3',5'-di-(alpha,alpha-dimethylbenzyl )azobenzene

Suppliers and Price of 2,4-Bis(1-methyl-1-phenylethyl)-6-((2-nitrophenyl)azo)phenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2,4-Bis(1-methyl-1-phenylethyl)-6-((2-nitrophenyl)azo)phenol

Chemical Property:

Vapor Pressure:1.2E-15mmHg at 25°C
Boiling Point:627.2°C at 760 mmHg
Flash Point:333.1°C
PSA：90.77000
Density:1.14g/cm³
LogP:8.89080
XLogP3:8.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:479.22089180
Heavy Atom Count:36
Complexity:749

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C1=CC=CC=C1)C2=CC(=C(C(=C2)N=NC3=CC=CC=C3[N+](=O)[O-])O)C(C)(C)C4=CC=CC=C4
Uses 2-((2-Nitrophenyl)diazenyl)-4,6-bis(2-phenylpropan-2-yl)phenol is an intermediate in the synthesis of Benzotriazole BT (B206990), a low volatile benzotriazole UV light absorber and stabilizer.

Technology Process of 2,4-Bis(1-methyl-1-phenylethyl)-6-((2-nitrophenyl)azo)phenol

There total 5 articles about 2,4-Bis(1-methyl-1-phenylethyl)-6-((2-nitrophenyl)azo)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2772-45-4,106060-52-0
2,4-di-cumylphenol

: 119-66-4
2-nitrobenzenediazonium chloride

: 70693-50-4
2-nitro-2'-hydroxy-3',5'-bis(α,α-dimethylbenzyl)azobenzene

Guidance literature:: With sodium hydroxide; In ethanol; at 10 ℃; for 3h;

Reference yield:

: 2772-45-4,106060-52-0
2,4-di-cumylphenol

: 119-66-4
2-nitrobenzenediazonium chloride

: 88-74-4
2-nitro-aniline

: 70693-50-4
2-Nitro-2'-hydroxy-3',5'-di(α,α-dimethylbenzyl)azobenzene Acid

Guidance literature:: With sodium nitrite; In methanol; concentrated aqueous hydrochloric acid; water;

Reference yield:

: 88-73-3
2-Chloronitrobenzene

: 70693-50-4
2-nitro-2'-hydroxy-3',5'-bis(α,α-dimethylbenzyl)azobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium hydroxide / 150 - 220 °C / 90009 - 150015 Torr

2: hydrogenchloride; sodium nitrite / water / 1 h / 10 °C

3: sodium hydroxide / ethanol / 3 h / 10 °C

With hydrogenchloride; ammonium hydroxide; sodium hydroxide; sodium nitrite; In ethanol; water;