Guanidine, (2-(hexahydro-1(2H)-azocinylmethyl)benzyl)-, sulfate

Base Information

Chemical Name:Guanidine, (2-(hexahydro-1(2H)-azocinylmethyl)benzyl)-, sulfate
CAS No.:115174-20-4
Molecular Formula:C16H28N4O4S
Molecular Weight:372.4829
Hs Code.:
DSSTox Substance ID:DTXSID70150980

Synonyms:o-Heptamethyleniminomethylbenzylguanidine sulfate;115174-20-4;Guanidine, (2-(hexahydro-1(2H)-azocinylmethyl)benzyl)-, sulfate;(2-(Hexahydro-1(2H)-azocinylmethyl)benzyl)guanidine sulfate;DTXSID70150980;LS-73693

Suppliers and Price of Guanidine, (2-(hexahydro-1(2H)-azocinylmethyl)benzyl)-, sulfate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Guanidine, (2-(hexahydro-1(2H)-azocinylmethyl)benzyl)-, sulfate

Chemical Property:

Vapor Pressure:1.45E-07mmHg at 25°C
Boiling Point:429°Cat760mmHg
Flash Point:213.3°C
Density:g/cm³
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:372.18312656
Heavy Atom Count:25
Complexity:372

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCCN(CCC1)CC2=CC=CC=C2CN=C(N)N.OS(=O)(=O)O

Technology Process of Guanidine, (2-(hexahydro-1(2H)-azocinylmethyl)benzyl)-, sulfate

There total 4 articles about Guanidine, (2-(hexahydro-1(2H)-azocinylmethyl)benzyl)-, sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 867-44-7,147895-43-0
S-Methylisothiourea sulfate

: 115174-14-6
o-Heptamethyleniminomethylbenzylamine

: 115174-20-4
o-Heptamethyleniminomethylbenzylguanidine sulphate

Guidance literature:: In water; for 20h; Heating;
DOI:10.1002/ardp.19883210202

Reference yield:

: 1121-92-2
heptamethyleneimine

: 115174-20-4
o-Heptamethyleniminomethylbenzylguanidine sulphate

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / toluene / 2 h / Heating

2: 50 percent / LiAlH₄ / diethyl ether / 3 h / Heating

3: 60 percent / H₂O / 20 h / Heating

With lithium aluminium tetrahydride; In diethyl ether; water; toluene;
DOI:10.1002/ardp.19883210202

Reference yield:

: 115174-11-3
o-Heptamethyleniminomethylbenzonitrile

: 115174-20-4
o-Heptamethyleniminomethylbenzylguanidine sulphate

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / LiAlH₄ / diethyl ether / 3 h / Heating

2: 60 percent / H₂O / 20 h / Heating

With lithium aluminium tetrahydride; In diethyl ether; water;
DOI:10.1002/ardp.19883210202