1,1-Dimethylsilinane-3,3-dicarboxylic acid

Base Information

• Chemical Name: 1,1-Dimethylsilinane-3,3-dicarboxylic acid
• CAS No.: 17864-77-6
• Molecular Formula: C9H16O4Si
• Molecular Weight: 216.3064
• NSC Number: 96829
• DSSTox Substance ID: DTXSID50294497
• Wikidata: Q82033838

Synonyms:17864-77-6;1,1-dimethylsilinane-3,3-dicarboxylic acid;NSC96829;NCIOpen2_006193;DTXSID50294497;NSC-96829

Chemical Property of 1,1-Dimethylsilinane-3,3-dicarboxylic acid

Chemical Property:

• Vapor Pressure: 1.25E-06mmHg at 25°C
• Boiling Point: 374.2°Cat760mmHg
• Flash Point: 180.1°C
• Density: 1.17g/cm³
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 216.08178552
• Heavy Atom Count: 14
• Complexity: 258

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Si]1(CCCC(C1)(C(=O)O)C(=O)O)C

Technology Process of 1,1-Dimethylsilinane-3,3-dicarboxylic acid

There total 2 articles about 1,1-Dimethylsilinane-3,3-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl(chloromethyl)(3-chloropropyl)silane (18209-77-3) → 1.1-Dimethyl-1-sila-cyclohexan-3.3-dicarbonsaeure (17864-77-6)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOEt, NaI / ethanol / Heating

2: aq. KOH

With potassium hydroxide; sodium ethanolate; sodium iodide; In ethanol;

DOI:10.1021/jm00336a002

Reference yield:

1,1-dimethyl-silinane-3,3-dicarboxylic acid diethyl ester (18401-42-8) → 1.1-Dimethyl-1-sila-cyclohexan-3.3-dicarbonsaeure (17864-77-6)

Guidance literature:

With potassium hydroxide;

DOI:10.1021/jm00336a002

upstream raw materials:

1,1-dimethyl-silinane-3,3-dicarboxylic acid diethyl ester

dimethyl(chloromethyl)(3-chloropropyl)silane

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