Piperidinium, 1-(1,3-dioxolan-2-ylmethyl)-4-hydroxy-1-methyl-, bromide benzilate, trans-

Base Information

Chemical Name:Piperidinium, 1-(1,3-dioxolan-2-ylmethyl)-4-hydroxy-1-methyl-, bromide benzilate, trans-
CAS No.:79708-67-1
Molecular Formula:Br*C₂₄H₃₀NO₅
Molecular Weight:492.41
Hs Code.:
DSSTox Substance ID:DTXSID901000680

Synonyms:Piperidinium, 1-(1,3-dioxolan-2-ylmethyl)-4-hydroxy-1-methyl-, bromide benzilate, trans-;trans-4-Benziloyloxy-1-(1,3-dioxolan-2-ylmethyl)-1-methylpiperidinium bromide;trans-1-(1,3-Dioxolan-2-ylmethyl)-4-hydroxy-1-methylpiperidinium bromide benzilate;79708-67-1;Piperidinium, 1-(1,3-dioxolan-2-ylmethyl)-4-((hydroxydiphenylacetyl)oxy)-1-methyl-, bromide, trans-;C24H30NO5.Br;C24-H30-N-O5.Br;DTXSID901000680;LS-116543;1-[(1,3-Dioxolan-2-yl)methyl]-4-{[hydroxy(diphenyl)acetyl]oxy}-1-methylpiperidin-1-ium bromide

Suppliers and Price of Piperidinium, 1-(1,3-dioxolan-2-ylmethyl)-4-hydroxy-1-methyl-, bromide benzilate, trans-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Piperidinium, 1-(1,3-dioxolan-2-ylmethyl)-4-hydroxy-1-methyl-, bromide benzilate, trans-

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:7
Exact Mass:491.13074
Heavy Atom Count:31
Complexity:538

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[N+]1(CCC(CC1)OC(=O)C(C2=CC=CC=C2)(C3=CC=CC=C3)O)CC4OCCO4.[Br-]

Technology Process of Piperidinium, 1-(1,3-dioxolan-2-ylmethyl)-4-hydroxy-1-methyl-, bromide benzilate, trans-

There total 2 articles about Piperidinium, 1-(1,3-dioxolan-2-ylmethyl)-4-hydroxy-1-methyl-, bromide benzilate, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 74-83-9
methyl bromide

: 91540-19-1
4-benziloyloxy-1-(1,3-dioxolan-2-ylmethyl)piperidine

: 79708-67-1
trans 4-benziloyloxy-1-(1,3-dioxolan-2-ylmethyl)-1-methylpiperidinium bromide

: 79708-68-2
cis 4-benziloyloxy-1-(1,3-dioxolan-2-ylmethyl)-1-methylpiperidinium bromide

Guidance literature:: In acetonitrile; for 12h; Ambient temperature;
DOI:10.1248/cpb.32.1126

Reference yield:

: 91540-18-0
1-(1,3-dioxolan-2-ylmethyl)-4-piperidinol

: 79708-67-1
trans 4-benziloyloxy-1-(1,3-dioxolan-2-ylmethyl)-1-methylpiperidinium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) oil, 80 deg C, 2.) 3 h

2: 44 percent / acetonitrile / 12 h / Ambient temperature

With sodium hydride; In acetonitrile;
DOI:10.1248/cpb.32.1126