3,6-dinitrobenzo(a)pyrene

Base Information

• Chemical Name: 3,6-dinitrobenzo(a)pyrene
• CAS No.: 128714-76-1
• Molecular Formula: C20H10N2O4
• Molecular Weight: 342.3044
• Mol file: 128714-76-1.mol

Synonyms:

Chemical Property of 3,6-dinitrobenzo(a)pyrene

Chemical Property:

• Vapor Pressure: 3.6E-13mmHg at 25°C
• Boiling Point: 587.6°Cat760mmHg
• Flash Point: 292.2°C
• PSA: 91.64000
• Density: 1.557g/cm³
• LogP: 6.60000

Purity/Quality:

99%min ^*data from raw suppliers

3,6-DINITROBENZO(A)PYRENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,6-dinitrobenzo(a)pyrene

There total 3 articles about 3,6-dinitrobenzo(a)pyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

benzopyrene (50-32-8,42299-33-2,34505-58-3) → 6-nitrobenzo(a)pyrene (63041-90-7) + 3-nitrobenzopyrene (70021-98-6) + 1-nitrobenzopyrene (70021-99-7) + 3,6-dinitrobenzo[a]pyrene (128714-76-1) + 1,6-dinitrobenzo[a]pyrene (128714-75-0)

Guidance literature:

With nitric acid; In acetic anhydride; for 0.5h; Product distribution; Ambient temperature; other reaction time;

DOI:10.1248/cpb.38.3158

Reference yield:

6-Nitro-benzo[def]chrysene-3-diazonium; hydrogen sulfate → 3,6-dinitrobenzo[a]pyrene (128714-76-1)

Guidance literature:

With copper(II) sulfate; sodium sulfite; sodium nitrite; In water; for 1h; Yield given;

DOI:10.1248/cpb.38.3158

Reference yield:

benzopyrene (50-32-8,42299-33-2,34505-58-3) → 6-nitrobenzo(a)pyrene (63041-90-7) + 3-nitrobenzopyrene (70021-98-6) + 1-nitrobenzopyrene (70021-99-7) + 3,6-dinitrobenzo[a]pyrene (128714-76-1)

Guidance literature:

With Nitrogen dioxide; Further Variations:; Reagents; irradiation; Product distribution;

DOI:10.1016/S0045-6535(00)00029-1

upstream raw materials:

benzopyrene

Refernces

• 1、 Fukuhara,Miyata,Matsui,Matsui,Ishidata Jr.,Kamiya. "Synthesis, chemical properties and mutagenicity of 1,6- and 3,6-dinitrobenzo[a]pyrenes". . p. 3158 - 3161. Retrieved 2007/10/02.