Isogomisin O

Base Information

• Chemical Name: Isogomisin O
• CAS No.: 83916-76-1
• Molecular Formula: C₂₃H₂₈O₇
• Molecular Weight: 416.471

Synonyms:exo-7-Methoxycarbonylbicycloheptanecarboxylate;endo-7-Methoxycarbonylbicyclo

Chemical Property of Isogomisin O

Chemical Property:

• Melting Point: 140 - 141 °C (hexane)
• Boiling Point: 570.3±50.0 °C(Predicted)
• PKA: 13.81±0.60(Predicted)
• PSA: 75.61000
• Density: 1.204±0.06 g/cm3(Predicted)
• LogP: 3.97840

Purity/Quality:

98%Min ^*data from raw suppliers

IsogomisinO ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Isogomisin O

There total 8 articles about Isogomisin O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(6R,7R,S-Biar)-7,8-dihydro-1,10,11,12-tetramethoxy-6,7-dimethyl-2,3-methylenedioxydibenzocycloocten-5(6H)-one → Deacetylkadsurin (51670-42-9,65167-73-9,83916-76-1)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 3h;

DOI:10.1016/0957-4166(94)00369-M

Reference yield:

angeloylisogomisin O (83864-70-4,140460-42-0,140461-47-8) → isogomisin O (51670-42-9,65167-73-9,83916-76-1)

Guidance literature:

With potassium hydroxide; In ethanol; at 70 - 73 ℃; for 6h;

Reference yield:

benzoylisogomisin O (83864-71-5) → isogomisin O (51670-42-9,65167-73-9,83916-76-1)

Guidance literature:

With potassium hydroxide; In ethanol; at 70 - 73 ℃; for 2h;

upstream raw materials:

diazomethane

C₂₁H₂₄O₇

kadsurin

kadsulignan H

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