2-(2-Amino-1-hydroxyethyl)dibenzofuran hydrochloride

Base Information

Chemical Name:2-(2-Amino-1-hydroxyethyl)dibenzofuran hydrochloride
CAS No.:63765-70-8
Molecular Formula:C₁₄H₁₃NO₂*ClH
Molecular Weight:263.724
Hs Code.:
DSSTox Substance ID:DTXSID80980290

Synonyms:63765-70-8;DTXSID80980290;Ethanol, 2-amino-1-(dibenzofuran-2''-yl)-, hydrochloride;2-Amino-1-(dibenzo[b,d]furan-3-yl)ethan-1-ol--hydrogen chloride (1/1)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-Amino-1-hydroxyethyl)dibenzofuran hydrochloride

Chemical Property:

Vapor Pressure:8.87E-09mmHg at 25°C
Boiling Point:447.1°Cat760mmHg
Flash Point:224.2°C
Density:g/cm³
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:263.0713064
Heavy Atom Count:18
Complexity:271

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3=C(O2)C=C(C=C3)C(CN)O.Cl

Technology Process of 2-(2-Amino-1-hydroxyethyl)dibenzofuran hydrochloride

There total 2 articles about 2-(2-Amino-1-hydroxyethyl)dibenzofuran hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.9%

: 96706-49-9
(2-dibenzofuranyl)-hydroxy-acetonitrile

: 63765-70-8
β-(2-dibenzofuranyl)-β-hydroxy-ethylamine hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; platinum(IV) oxide; In methanol; ethanol; for 8h; under 2585.7 Torr; Ambient temperature;
DOI:10.1016/0223-5234(87)90270-4

Reference yield:

: 5397-82-0
dibenzofuran-2-carbaldehyde

: 63765-70-8
β-(2-dibenzofuranyl)-β-hydroxy-ethylamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 92.8 percent / glacial acetic / diethyl ether / cooling, then room temp.

2: 82.9 percent / H₂, HCl / PtO₂ / ethanol; methanol / 8 h / 2585.7 Torr / Ambient temperature

With hydrogenchloride; hydrogen; acetic acid; platinum(IV) oxide; In methanol; diethyl ether; ethanol;
DOI:10.1016/0223-5234(87)90270-4