(2S)-2-amino-2-phenylacetyl chloride;hydrochloride

Base Information

Chemical Name:(2S)-2-amino-2-phenylacetyl chloride;hydrochloride
CAS No.:5321-31-3
Molecular Formula:C₈H₈ClNO*ClH
Molecular Weight:206.072
Hs Code.:
European Community (EC) Number:226-181-8
DSSTox Substance ID:DTXSID00892164
Mol file:5321-31-3.mol

Synonyms:5321-31-3;SCHEMBL2003210;DTXSID00892164

Suppliers and Price of (2S)-2-amino-2-phenylacetyl chloride;hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of (2S)-2-amino-2-phenylacetyl chloride;hydrochloride

Chemical Property:

Boiling Point:247.2°Cat760mmHg
Flash Point:103.3°C
Density:g/cm³
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:205.0061193
Heavy Atom Count:12
Complexity:143

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(C(=O)Cl)N.Cl
Isomeric SMILES:C1=CC=C(C=C1)[C@@H](C(=O)Cl)N.Cl

Technology Process of (2S)-2-amino-2-phenylacetyl chloride;hydrochloride

There total 2 articles about (2S)-2-amino-2-phenylacetyl chloride;hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2935-35-5
(S)-2-phenylglycine

: 5321-31-3
phenylglycidylchloride hydrochloride

Guidance literature:: With thionyl chloride; In diethyl ether; at -10 ℃;
DOI:10.1016/S0040-4039(00)76640-8

Reference yield:

: 875-74-1
(R)-phenylglycine

: 39878-87-0,5321-31-3
d(-)-alpha-phenylglycine chloride hydrochloride

Guidance literature:: With thionyl chloride; In diethyl ether; at -10 ℃;
DOI:10.1016/S0040-4039(00)76640-8

Reference yield: 62.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: cobalt(II) chloride hexahydrate

: 118757-82-7
dichlorobis(imidazole)dimethyltin

: 7732-18-5
water

: 5321-31-3
phenylglycidylchloride hydrochloride

: ((C₃H₃N₂)2(CH₃)2SnCl₂)Co(H₂O)(C₆H₅CH(NH₂)COCl)*HCl

Guidance literature:: In methanol; MeOH soln. of CoCl2 added dropwise to MeOH soln. of ligand, stirred for 3 h, MeOH soln. of Sn compd. added (1:1:1 molar ratio), mixt. refluxed for 8 h; cooled to room temp., crystd. on storage, septd., washed (CHCl3), dried (vac.), elem. anal.;
DOI:10.1016/j.jorganchem.2012.04.027