Benzaldehyde, 4-ethyl-, oxime (9CI)

Base Information

• Chemical Name: Benzaldehyde, 4-ethyl-, oxime (9CI)
• CAS No.: 61946-88-1
• Molecular Formula: C9H11 N O
• Molecular Weight: 149.18974
• Hs Code.: 2928000090
• Mol file: 61946-88-1.mol

Synonyms:4-Ethylbenzaldoxime

Chemical Property of Benzaldehyde, 4-ethyl-, oxime (9CI)

Chemical Property:

• Vapor Pressure: 0.0329mmHg at 25°C
• Boiling Point: 232.4°C at 760 mmHg
• PKA: 10.81±0.10(Predicted)
• Flash Point: 128.4°C
• PSA: 32.59000
• Density: 0.99g/cm³
• LogP: 2.05710

Purity/Quality:

98%Min ^*data from raw suppliers

4-ETHYLBENZALDEHYDE OXIME 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzaldehyde, 4-ethyl-, oxime (9CI)

There total 1 articles about Benzaldehyde, 4-ethyl-, oxime (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-ethylbenzylaldehyde (4748-78-1) → N-[(E)-(4-ethylphenyl)methylidene]hydroxylamine (61946-88-1)

Guidance literature:

With hydroxylamine hydrochloride; sodium hydroxide; In ethanol; water; at 90 ℃;

DOI:10.1039/d0nj03474f

Reference yield: 73.0%

N-[(E)-(4-ethylphenyl)methylidene]hydroxylamine (61946-88-1) → 4-ethyl-N-hydroxybenzene-1-carboximidoyl chloride (61946-91-6)

Guidance literature:

With N-chloro-succinimide; In N,N-dimethyl-formamide; at 60 ℃;

DOI:10.1039/d0nj03474f

Reference yield:

N-[(E)-(4-ethylphenyl)methylidene]hydroxylamine (61946-88-1) → N-[(4-ethylphenyl)(morpholin-4-yl)methylidene]hydroxylamine

Guidance literature:

Multi-step reaction with 2 steps

1: N-chloro-succinimide / N,N-dimethyl-formamide / 60 °C

2: triethylamine / dichloromethane / 0 °C

With N-chloro-succinimide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1039/d0nj03474f

upstream raw materials:

4-ethylbenzylaldehyde

Downstream raw materials:

4-ethyl-N-hydroxybenzene-1-carboximidoyl chloride