3-[2-(1,1,1,3,3,3-hexafluoropropan-2-yl)-4-(1,1,1,3,3,3-hexafluoropropan-2-ylidene)-1,3-dithietan-2-yl]-2,5-dimethyl-7lambda~4~-[1,2]dithiolo[1,5-b][1,2]dithiole

Base Information

• Chemical Name: 3-[2-(1,1,1,3,3,3-hexafluoropropan-2-yl)-4-(1,1,1,3,3,3-hexafluoropropan-2-ylidene)-1,3-dithietan-2-yl]-2,5-dimethyl-7lambda~4~-[1,2]dithiolo[1,5-b][1,2]dithiole
• CAS No.: 66172-14-3
• Molecular Formula: C15H8F12S5
• Molecular Weight: 576.5299

Synonyms:

Chemical Property of 3-[2-(1,1,1,3,3,3-hexafluoropropan-2-yl)-4-(1,1,1,3,3,3-hexafluoropropan-2-ylidene)-1,3-dithietan-2-yl]-2,5-dimethyl-7lambda~4~-[1,2]dithiolo[1,5-b][1,2]dithiole

Chemical Property:

• Density: 1.81g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3-[2-(1,1,1,3,3,3-hexafluoropropan-2-yl)-4-(1,1,1,3,3,3-hexafluoropropan-2-ylidene)-1,3-dithietan-2-yl]-2,5-dimethyl-7lambda~4~-[1,2]dithiolo[1,5-b][1,2]dithiole

There total 2 articles about 3-[2-(1,1,1,3,3,3-hexafluoropropan-2-yl)-4-(1,1,1,3,3,3-hexafluoropropan-2-ylidene)-1,3-dithietan-2-yl]-2,5-dimethyl-7lambda~4~-[1,2]dithiolo[1,5-b][1,2]dithiole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

bis(trifluoromethyl)thioketene (7445-60-5) + 2,5-dimethyl-7λ4-[1,2]dithiolo[1,5-b][1,2]dithiole (2080-35-5) → 2,5-Dimethyl-3-[2-(2,2,2-trifluoro-1-trifluoromethyl-ethyl)-4-(2,2,2-trifluoro-1-trifluoromethyl-ethylidene)-[1,3]dithietan-2-yl]-7λ4-[1,2]dithiolo[1,5-b][1,2]dithiole (66172-14-3)

Guidance literature:

In dichloromethane; ratio of thiothiophene and bis(trifluoromethylthioketene) 1:2, 22h;

DOI:10.1021/jo00406a047

Reference yield:

→ 2,5-Dimethyl-3-[2-(2,2,2-trifluoro-1-trifluoromethyl-ethyl)-4-(2,2,2-trifluoro-1-trifluoromethyl-ethylidene)-[1,3]dithietan-2-yl]-7λ4-[1,2]dithiolo[1,5-b][1,2]dithiole (66172-14-3)

Guidance literature:

Thiothiophthen 26, Bis(trifluormethyl)thioketen ;

DOI:10.1021/jo00406a047

upstream raw materials:

bis(trifluoromethyl)thioketene

2,5-dimethyl-7λ⁴-[1,2]dithiolo[1,5-b][1,2]dithiole

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