o-((p-(Dimethylamino)phenyl)azo)phenol

Base Information

• Chemical Name: o-((p-(Dimethylamino)phenyl)azo)phenol
• CAS No.: 6396-84-5
• Molecular Formula: C₁₄H₁₅N₃O
• Molecular Weight: 241.293
• Mol file: 6396-84-5.mol

Synonyms:o-((p-(Dimethylamino)phenyl)azo)phenol;Phenol, o-((p-(dimethylamino)phenyl)azo)-;6396-84-5;Phenol, o-[[p-(dimethylamino)phenyl]azo]-;2'-hydroxy-4-dimethylamino azobenzene;Phenol, 2-[[4-(dimethylamino)phenyl]azo]-

Chemical Property of o-((p-(Dimethylamino)phenyl)azo)phenol

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 406.452°C at 760 mmHg
• Flash Point: 199.616°C
• Density: 1.113g/cm³
• XLogP3: 3.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 241.121512110
• Heavy Atom Count: 18
• Complexity: 272

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=CC=C(C=C1)N=NC2=CC=CC=C2O

Technology Process of o-((p-(Dimethylamino)phenyl)azo)phenol

There total 3 articles about o-((p-(Dimethylamino)phenyl)azo)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

4-(phenyl-NNO-azoxy)-N,N-dimethylaniline (3291-89-2,93830-75-2) → 2-(4-Dimethylamino-phenylazo)-phenol (6396-84-5) + 4-(phenyl-ONN-azoxy)-N,N-dimethylaniline (13921-71-6)

Guidance literature:

In benzene; for 7h; Irradiation;

DOI:10.1021/jo00351a018

Reference yield:

2-aminophenyl p-toluenesulfonate (1216-96-2) → 2-(4-Dimethylamino-phenylazo)-phenol (6396-84-5)

Guidance literature:

Diazotization_.dann mit N.N-Dimethyl-anilin und anschliessenden Behandlung mit aethanol.Natronlauge;

DOI:10.1084/jem.87.2.139

Reference yield:

→ 2-(4-Dimethylamino-phenylazo)-phenol (6396-84-5)

Guidance literature:

α-p-Dimethylamino-azooxybenzol-N-oxid 5, H2SO4 (80-100percent), 40-80grad erwaermen;

upstream raw materials:

2-aminophenyl p-toluenesulfonate

4-(phenyl-NNO-azoxy)-N,N-dimethylaniline