Technology Process of Benzoic acid, 2-hydroxy-6-(8,11-pentadecadienyl)-, (Z,Z)-
There total 45 articles about Benzoic acid, 2-hydroxy-6-(8,11-pentadecadienyl)-, (Z,Z)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
ethanol;
for 6h;
Heating;
DOI:10.1248/cpb.49.18
- Guidance literature:
-
With
aluminium(III) iodide; (+)-limonene;
In
carbon disulfide;
1.) r.t., 10 min, 2.) reflux, 30 min;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere; Schlenk technique
2.1: tetrabutyl-ammonium chloride; palladium diacetate; lithium chloride; lithium acetate / N,N-dimethyl acetamide / 3 h / 70 °C / Inert atmosphere; Schlenk technique; Sealed tube
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C / Inert atmosphere; Schlenk technique
3.2: 1 h / -78 - 20 °C / Inert atmosphere; Schlenk technique
4.1: potassium hydroxide / water; 1,4-dioxane / 18 h / 55 °C / Inert atmosphere; Schlenk technique
With
pyridine; n-butyllithium; lithium acetate; tetrabutyl-ammonium chloride; palladium diacetate; lithium chloride; potassium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; N,N-dimethyl acetamide; water;
2.1: |Heck Reaction / 3.1: |Wittig Olefination / 3.2: |Wittig Olefination;
DOI:10.1021/acs.orglett.8b02705