1,4,4-Trimethyl-2,3-diazabicyclo-(3,2,2)-non-2-ene-2,3-dioxide

Base Information

• Chemical Name: 1,4,4-Trimethyl-2,3-diazabicyclo-(3,2,2)-non-2-ene-2,3-dioxide
• CAS No.: 34122-40-2
• Molecular Formula: C10H18 N2 O2
• Molecular Weight: 198.265
• Hs Code.: 2933990090
• European Community (EC) Number: 251-833-3
• Wikidata: Q81994467
• Mol file: 34122-40-2.mol

Synonyms:34122-40-2;2,3-Diazabicyclo(3.2.2)non-2-ene, 1,4,4-trimethyl-, 2,3-dioxide;2,3-Diazabicyclo[3.2.2]non-2-ene, 1,4,4-trimethyl-, 2,3-dioxide;SCHEMBL16637962;EINECS 251-833-3;1,4,4-Trimethyl-2,3-diazabicyclo-(3,2,2)-non-2-ene-2,3-dioxide;FT-0606749;1,4,4-Trimethyl-2,3-diazabicyclo[3.2.2]non-2-ene 2,3-dioxide

Chemical Property of 1,4,4-Trimethyl-2,3-diazabicyclo-(3,2,2)-non-2-ene-2,3-dioxide

Chemical Property:

• Vapor Pressure: 8.131hPa at 21.1℃
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 57.50000
• Density: g/cm³
• LogP: 2.11790
• Water Solubility.: 3.172g/L at 20℃
• XLogP3: 1.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 198.136827821
• Heavy Atom Count: 14
• Complexity: 267

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(C2CCC(CC2)(N([N+]1=O)[O-])C)C

Technology Process of 1,4,4-Trimethyl-2,3-diazabicyclo-(3,2,2)-non-2-ene-2,3-dioxide

There total 2 articles about 1,4,4-Trimethyl-2,3-diazabicyclo-(3,2,2)-non-2-ene-2,3-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2,3-diazabicyclo<3.2.2>non-2-ene N,N'-dioxide (34122-40-2)

Guidance literature:

p-Menthan-diamin (1), MCPBA/CH2Cl2/CaCO3;

DOI:10.1016/0040-4020(75)80312-7

Reference yield:

→ 1,4,4-trimethyl-2,3-diaza-bicyclo[3.2.2]non-2-ene 2,3-dioxide (34122-40-2)

Guidance literature:

cis/trans-4-(1-Amino-1-methylethyl)-1-methylcyclohexylamin, H2O2/Na2WO4;

DOI:10.1021/jo00898a007

Reference yield:

1,4,4-trimethyl-2,3-diaza-bicyclo[3.2.2]non-2-ene 2,3-dioxide (34122-40-2) → (Z)-1,8-dinitro-p-menthane (54166-26-6)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In benzene;

DOI:10.1021/jo00898a007

Downstream raw materials:

(Z)-1,8-dinitro-p-menthane

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